Technology Process of C32H34ClN3O6
There total 5 articles about C32H34ClN3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C24H19ClO7; C8H17N3*2ClH;
With
sodium acetate;
In
tetrahydrofuran;
at -20 ℃;
for 1h;
Inert atmosphere;
With
acetic acid;
In
tetrahydrofuran;
for 1h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; sodium cyanoborohydride / water; methanol / 1.5 h / 20 °C / pH 4 / Inert atmosphere; Cooling with ice
2.1: methanol; hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere
3.1: sodium acetate / tetrahydrofuran / 1 h / -20 °C / Inert atmosphere
3.2: 1 h / Inert atmosphere; Reflux
With
hydrogenchloride; methanol; sodium acetate; sodium cyanoborohydride;
In
tetrahydrofuran; 1,4-dioxane; methanol; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diisobutylaluminium hydride / toluene / 0.83 h / -78 °C / Inert atmosphere
2.1: water; toluene; methanol / 20 °C / Inert atmosphere
3.1: hydrogenchloride; sodium cyanoborohydride / water; methanol / 1.5 h / 20 °C / pH 4 / Inert atmosphere; Cooling with ice
4.1: methanol; hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere
5.1: sodium acetate / tetrahydrofuran / 1 h / -20 °C / Inert atmosphere
5.2: 1 h / Inert atmosphere; Reflux
With
hydrogenchloride; methanol; sodium acetate; diisobutylaluminium hydride; sodium cyanoborohydride;
In
tetrahydrofuran; 1,4-dioxane; methanol; water; toluene;