4-(4-nitrophenyl)piperazinium 4-(4-nitrophenyl)piperazine-1-carbodithioate

Base Information

Chemical Name:4-(4-nitrophenyl)piperazinium 4-(4-nitrophenyl)piperazine-1-carbodithioate
CAS No.:1169605-02-0
Molecular Formula:C₁₀H₁₃N₃O₂*C₁₁H₁₃N₃O₂S₂
Molecular Weight:490.607
Hs Code.:

Synonyms:4-(4-nitrophenyl)piperazinium 4-(4-nitrophenyl)piperazine-1-carbodithioate

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Chemical Property of 4-(4-nitrophenyl)piperazinium 4-(4-nitrophenyl)piperazine-1-carbodithioate

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Technology Process of 4-(4-nitrophenyl)piperazinium 4-(4-nitrophenyl)piperazine-1-carbodithioate

There total 1 articles about 4-(4-nitrophenyl)piperazinium 4-(4-nitrophenyl)piperazine-1-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 75-15-0,12122-00-8
carbon disulfide

: 6269-89-2
1-(4-Nitrophenyl)piperazine

: 1169605-02-0
4-(4-nitrophenyl)piperazinium 4-(4-nitrophenyl)piperazine-1-carbodithioate

Guidance literature:: In methanol; at 0 ℃; for 4h;
DOI:10.1016/j.jorganchem.2009.01.047

Reference yield: 77.0%

: 1169605-02-0
4-(4-nitrophenyl)piperazinium 4-(4-nitrophenyl)piperazine-1-carbodithioate

: 683-18-1
dibutyltin chloride

: 946151-58-2
chlorobis(n-butyl)(4-(4-nitrophenyl)piperazine-1-carbodithioato)tin(IV)

Guidance literature:: In methanol; byproducts: 4-(4-nitrophenyl)piperazinium chloride; mixt. of Sn compd. and piperazinium salt (molar ratio = 1:1) in dry MeOHrefluxed for 6 h under stirring; ppt. filtered off, recrystd. from CHCl3/EtOH; elem. anal.;
DOI:10.1016/j.jorganchem.2009.01.047

Reference yield: 73.0%

: 1169605-02-0
4-(4-nitrophenyl)piperazinium 4-(4-nitrophenyl)piperazine-1-carbodithioate

: 1135-99-5
diphenyltin(IV) dichloride

: 1169605-01-9
bis(phenyl)bis(4-(4-nitrophenyl)piperazine-1-carbodithioato)tin(IV)

Guidance literature:: In methanol; byproducts: 4-(4-nitrophenyl)piperazinium chloride; mixt. of Ph2SnCl2 and piperazinium salt (molar ratio = 1:2) in dry MeOH refluxed for 6 h under stirring; ppt. filtered off, recrystd. from CHCl3/EtOH; elem. anal.;
DOI:10.1016/j.jorganchem.2009.01.047