2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

Base Information

Chemical Name:2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside
CAS No.:82305-37-1
Molecular Formula:C₅₄H₅₄O₁₁
Molecular Weight:879.016
Hs Code.:

Synonyms:2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

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Chemical Property of 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

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Technology Process of 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

There total 5 articles about 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 18929-82-3
4,6-O-benzylidene-α-D-glucopyranosyl-(1→1)-4',6'-O-benzylidene-α-D-glucopyranoside

: 100-39-0
benzyl bromide

: 82305-37-1
2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2007.05.009

Reference yield:

: 99-20-7
TREHALOSE

: 82305-37-1
2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / p-toluenesulfonic acid monohydrate / dimethylformamide / 2 h / 65 °C / 40 Torr / reflux

2: 1.) 50percent NaH / 1.) DMSO, 1 h, r.t.; 2.) DMSO, 2 h

With sodium hydride; toluene-4-sulfonic acid; In N,N-dimethyl-formamide;

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 82305-37-1
2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / p-toluenesulfonic acid monohydrate / dimethylformamide / 2 h / 65 °C / 40 Torr / reflux

2: 1.) 50percent NaH / 1.) DMSO, 1 h, r.t.; 2.) DMSO, 2 h

With sodium hydride; toluene-4-sulfonic acid; In N,N-dimethyl-formamide;