4-(2-phenylethyl)piperidine-1,4-dicarboxylic acid 4-ethyl 1-tert-butyl diester

Base Information

Chemical Name:4-(2-phenylethyl)piperidine-1,4-dicarboxylic acid 4-ethyl 1-tert-butyl diester
CAS No.:152830-59-6
Molecular Formula:C₂₁H₃₁NO₄
Molecular Weight:361.481
Hs Code.:

Synonyms:4-(2-phenylethyl)piperidine-1,4-dicarboxylic acid 4-ethyl 1-tert-butyl diester

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Chemical Property of 4-(2-phenylethyl)piperidine-1,4-dicarboxylic acid 4-ethyl 1-tert-butyl diester

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Technology Process of 4-(2-phenylethyl)piperidine-1,4-dicarboxylic acid 4-ethyl 1-tert-butyl diester

There total 3 articles about 4-(2-phenylethyl)piperidine-1,4-dicarboxylic acid 4-ethyl 1-tert-butyl diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1126-09-6
4-carbethoxypiperidine

: 152830-59-6
4-(2-phenylethyl)piperidine-1,4-dicarboxylic acid 4-ethyl 1-tert-butyl diester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NaOH / tetrahydrofuran / 22 h / Heating

2: 1.) lithium diisopropylamide / 1.) THF, hexane, -70 deg C, 1 h, 2.) THF, hexane, RT, 22 h

With sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/jm00029a008

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 152830-59-6
4-(2-phenylethyl)piperidine-1,4-dicarboxylic acid 4-ethyl 1-tert-butyl diester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NaOH / tetrahydrofuran / 22 h / Heating

2: 1.) lithium diisopropylamide / 1.) THF, hexane, -70 deg C, 1 h, 2.) THF, hexane, RT, 22 h

With sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/jm00029a008

Reference yield:

: 103-63-9
1-phenyl-2-bromoethane

: 142851-03-4
1-tert-butyl 4-ethyl piperidine-1,4-dicarboxylate

: 152830-59-6
4-(2-phenylethyl)piperidine-1,4-dicarboxylic acid 4-ethyl 1-tert-butyl diester

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, hexane, -70 deg C, 1 h, 2.) THF, hexane, RT, 22 h;
DOI:10.1021/jm00029a008