di-tert-butyl 4-benzoyl-L-glutamate

Base Information

Chemical Name:di-tert-butyl 4-benzoyl-L-glutamate
CAS No.:123724-57-2
Molecular Formula:C₂₄H₃₆Cl₂N₂O₅
Molecular Weight:503.466
Hs Code.:

di-tert-butyl 4-<bis(2-chloroethyl)amino>benzoyl-L-glutamate

Synonyms:di-tert-butyl 4-benzoyl-L-glutamate

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Chemical Property of di-tert-butyl 4-benzoyl-L-glutamate

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Technology Process of di-tert-butyl 4-benzoyl-L-glutamate

There total 3 articles about di-tert-butyl 4-benzoyl-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 0.3%

: 123724-54-9
di-tert-butyl 4-benzoyl-L-glutamate

: 124-63-0
methanesulfonyl chloride

: 123724-57-2
di-tert-butyl 4-benzoyl-L-glutamate

: 123724-56-1
di-tert-butyl 4-<(2-chloroethyl)<2-(mesyloxy)ethyl>amino>benzoyl-L-glutamate

Guidance literature:: With pyridine; 1.) 2 deg C, 20 min, 2.) 80 deg C, 80 min;
DOI:10.1021/jm00164a034

Reference yield:

: 32677-01-3
L-glutamic acid di-tert-butyl ester hydrochloride

: 123724-57-2
di-tert-butyl 4-benzoyl-L-glutamate

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂

2: H₂ / 10percent Pd/C

3: 78 percent / acetic acid / 48 h / Ambient temperature

4: 77 percent / pyridine / 1.) 2 deg C, 20 min, 2.) 80 deg C, 80 min

With pyridine; hydrogen; acetic acid; triethylamine; palladium on activated charcoal; In dichloromethane;
DOI:10.1021/jm00164a034

Reference yield:

: 76282-66-1
di-tert-butyl (S)-N-(p-aminobenzoyl)-glutamate

: 123724-57-2
di-tert-butyl 4-benzoyl-L-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / acetic acid / 48 h / Ambient temperature

2: 77 percent / pyridine / 1.) 2 deg C, 20 min, 2.) 80 deg C, 80 min

With pyridine; acetic acid;
DOI:10.1021/jm00164a034