2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-N-isopropyl-2-(2-methoxy-4-thiophen-2'-yl-phenyl)acetamide

Base Information

Chemical Name:2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-N-isopropyl-2-(2-methoxy-4-thiophen-2'-yl-phenyl)acetamide
CAS No.:1173004-49-3
Molecular Formula:C₂₆H₂₂F₁₇NO₂S₂
Molecular Weight:767.571
Hs Code.:

Synonyms:2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-N-isopropyl-2-(2-methoxy-4-thiophen-2'-yl-phenyl)acetamide

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Chemical Property of 2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-N-isopropyl-2-(2-methoxy-4-thiophen-2'-yl-phenyl)acetamide

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Technology Process of 2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-N-isopropyl-2-(2-methoxy-4-thiophen-2'-yl-phenyl)acetamide

There total 1 articles about 2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-N-isopropyl-2-(2-methoxy-4-thiophen-2'-yl-phenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 6165-68-0
thiophene boronic acid

: 1173004-38-0
rac-2-(4-bromo-2-methoxy-phenyl)-2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decylsulfanyl)-N-iso-propylacetamide

: 1173004-49-3
2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-N-isopropyl-2-(2-methoxy-4-thiophen-2'-yl-phenyl)acetamide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; at 90 ℃; for 18h; Inert atmosphere;
DOI:10.1039/b904577e

Reference yield:

: 1173004-49-3
2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-N-isopropyl-2-(2-methoxy-4-thiophen-2'-yl-phenyl)acetamide

: 100-39-0
benzyl bromide

: 1173004-60-8
N-isopropyl-2-(2-methoxy-5-thiophen-2'-yl-phenyl)-3-phenyl-propionamide

Guidance literature:: 2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-N-isopropyl-2-(2-methoxy-4-thiophen-2'-yl-phenyl)acetamide; benzyl bromide; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; Inert atmosphere; Reflux;

With samarium diiodide; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/b904577e