rac-2-(4-bromo-2-methoxy-phenyl)-2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decylsulfanyl)-N-iso-propylacetamide

Base Information

• Chemical Name: rac-2-(4-bromo-2-methoxy-phenyl)-2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decylsulfanyl)-N-iso-propylacetamide
• CAS No.: 1173004-38-0
• Molecular Formula: C₂₂H₁₉BrF₁₇NO₂S
• Molecular Weight: 764.341

Synonyms:rac-2-(4-bromo-2-methoxy-phenyl)-2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decylsulfanyl)-N-iso-propylacetamide

Chemical Property of rac-2-(4-bromo-2-methoxy-phenyl)-2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decylsulfanyl)-N-iso-propylacetamide

Chemical Property:

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Technology Process of rac-2-(4-bromo-2-methoxy-phenyl)-2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decylsulfanyl)-N-iso-propylacetamide

There total 1 articles about rac-2-(4-bromo-2-methoxy-phenyl)-2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decylsulfanyl)-N-iso-propylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H16BrNO3 (1173004-33-5) + 1H,1H,2H,2H-Perfluorodecanethiol (34143-74-3) → rac-2-(4-bromo-2-methoxy-phenyl)-2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decylsulfanyl)-N-iso-propylacetamide (1173004-38-0)

Guidance literature:

C₁₃H₁₆BrNO₃; 1H,1H,2H,2H-Perfluorodecanethiol; In dichloromethane; at 20 ℃; Inert atmosphere;

With trifluoroacetic anhydride; In dichloromethane; at 20 ℃; for 1h; Further stages; Inert atmosphere;

DOI:10.1039/b904577e

Reference yield: 100.0%

rac-2-(4-bromo-2-methoxy-phenyl)-2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decylsulfanyl)-N-iso-propylacetamide (1173004-38-0) + trimethylsilylacetylene (1066-54-2) → 2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-N-isopropyl-2-(2-methoxy-4-trimethylsilanylethynyl-phenyl)acetamide (1173004-46-0)

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In toluene; at 110 ℃; for 18h; Inert atmosphere;

DOI:10.1039/b904577e

Reference yield: 77.0%

rac-2-(4-bromo-2-methoxy-phenyl)-2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decylsulfanyl)-N-iso-propylacetamide (1173004-38-0) → (4-bromo-2-methoxy-phenyl)-N-iso-propylacetamide (1173004-53-9)

Guidance literature:

With samarium diiodide; In tetrahydrofuran; at 20 ℃; for 20h; Inert atmosphere;

DOI:10.1039/b904577e

upstream raw materials:

C₁₃H₁₆BrNO₃

1H,1H,2H,2H-Perfluorodecanethiol

Downstream raw materials:

2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-N-isopropyl-2-(2-methoxy-4-thiophen-2'-yl-phenyl)acetamide

(4-bromo-2-methoxy-phenyl)-N-iso-propylacetamide

rac-2-benzyl-2-(4-bromo-2-methoxy-phenyl)-N-iso-propylacetamide

2-benzyl-2-(4-bromo-2-methoxyphenyl)-2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-pent-4-enoic acid isopropylacetamide

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