(Z)-methyl N'-cyano-N-(3,5-dichloro-4-cyclopropylphenyl)carbamimidothioate

Base Information

Chemical Name:(Z)-methyl N'-cyano-N-(3,5-dichloro-4-cyclopropylphenyl)carbamimidothioate
CAS No.:1533434-94-4
Molecular Formula:C₁₂H₁₁Cl₂N₃S
Molecular Weight:300.211
Hs Code.:

Synonyms:(Z)-methyl N'-cyano-N-(3,5-dichloro-4-cyclopropylphenyl)carbamimidothioate

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Chemical Property of (Z)-methyl N'-cyano-N-(3,5-dichloro-4-cyclopropylphenyl)carbamimidothioate

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Technology Process of (Z)-methyl N'-cyano-N-(3,5-dichloro-4-cyclopropylphenyl)carbamimidothioate

There total 4 articles about (Z)-methyl N'-cyano-N-(3,5-dichloro-4-cyclopropylphenyl)carbamimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 420-04-2
CYANAMID

: 1533425-18-1
1,3-dichloro-2-cyclopropyl-5-isothiocyanatobenzene

: 74-88-4
methyl iodide

: 1533434-94-4
(Z)-methyl N'-cyano-N-(3,5-dichloro-4-cyclopropylphenyl)carbamimidothioate

Guidance literature:: CYANAMID; With sodium methylate; In methanol; at 20 ℃; for 0.5h; under 760.051 Torr; Inert atmosphere;

1,3-dichloro-2-cyclopropyl-5-isothiocyanatobenzene; In methanol; toluene; for 2h; under 760.051 Torr; Inert atmosphere;

methyl iodide; In methanol; toluene; at 20 ℃; under 760.051 Torr; Inert atmosphere;

Reference yield:

: 1533425-16-9
1,3-dichloro-2-cyclopropyl-5-nitrobenzene

: 1533434-94-4
(Z)-methyl N'-cyano-N-(3,5-dichloro-4-cyclopropylphenyl)carbamimidothioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: iron; ammonium chloride / methanol; water / 2 h / 760.05 Torr / Inert atmosphere; Reflux

2.1: dichloromethane / 20 °C / 760.05 Torr / Inert atmosphere

3.1: sodium methylate / methanol / 0.5 h / 20 °C / 760.05 Torr / Inert atmosphere

3.2: 2 h / 760.05 Torr / Inert atmosphere

3.3: 20 °C / 760.05 Torr / Inert atmosphere

With sodium methylate; iron; ammonium chloride; In methanol; dichloromethane; water;

Reference yield:

: 1533425-17-0
3,5-dichloro-4-cyclopropylaniline

: 1533434-94-4
(Z)-methyl N'-cyano-N-(3,5-dichloro-4-cyclopropylphenyl)carbamimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 20 °C / 760.05 Torr / Inert atmosphere

2.1: sodium methylate / methanol / 0.5 h / 20 °C / 760.05 Torr / Inert atmosphere

2.2: 2 h / 760.05 Torr / Inert atmosphere

2.3: 20 °C / 760.05 Torr / Inert atmosphere

With sodium methylate; In methanol; dichloromethane;