6-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-naphthalenecarboxylic acid methyl ester

Base Information

Chemical Name:6-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-naphthalenecarboxylic acid methyl ester
CAS No.:1072710-71-4
Molecular Formula:C₂₈H₂₈O₃Si
Molecular Weight:440.614
Hs Code.:

Synonyms:6-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-naphthalenecarboxylic acid methyl ester

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Chemical Property of 6-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-naphthalenecarboxylic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 6-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-naphthalenecarboxylic acid methyl ester

There total 1 articles about 6-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-naphthalenecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90162-13-3
methyl 6-hydroxy-1-naphthoate

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1072710-71-4
6-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-naphthalenecarboxylic acid methyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 641571-11-1
3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)aniline

: 1072710-71-4
6-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-naphthalenecarboxylic acid methyl ester

: 1072710-70-3
6-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-N-[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]-1-naphthalenecarboxamide

Guidance literature:: 3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)aniline; With trimethylaluminum; In toluene; at 40 ℃; for 0.75h;

6-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-naphthalenecarboxylic acid methyl ester; In toluene; at 100 ℃; for 1.5h;

Reference yield:

: 1072710-71-4
6-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-naphthalenecarboxylic acid methyl ester

: 1072711-03-5
6-[(6-amino-pyridin-4-yl)oxy]-naphthalene-1-carboxylic acid [3-(4-methyl-imidazol-1-yl)-5-trifluoromethyl-phenyl]-amide

Guidance literature:: Multi-step reaction with 5 steps

1.1: trimethylaluminum / toluene / 0.75 h / 40 °C

1.2: 1.5 h / 100 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

3.1: potassium carbonate / dimethyl sulfoxide / 1 h / 55 °C

4.1: caesium carbonate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 90 °C

5.1: hydrogenchloride; water / ethanol / 5 h / 100 °C

With hydrogenchloride; tetrabutyl ammonium fluoride; water; trimethylaluminum; potassium carbonate; caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; ethanol; dimethyl sulfoxide; toluene;