(2S,4S,5R)-4-Methyl-5-phenyl-3-p-toluenesulfonyl-2-<(1S,2R)-1-hydroxy-2-carbomethoxy>propyloxazolidine

Base Information

Chemical Name:(2S,4S,5R)-4-Methyl-5-phenyl-3-p-toluenesulfonyl-2-<(1S,2R)-1-hydroxy-2-carbomethoxy>propyloxazolidine
CAS No.:129611-60-5
Molecular Formula:C₂₂H₂₇NO₆S
Molecular Weight:433.525
Hs Code.:

Synonyms:(2S,4S,5R)-4-Methyl-5-phenyl-3-p-toluenesulfonyl-2-<(1S,2R)-1-hydroxy-2-carbomethoxy>propyloxazolidine

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Chemical Property of (2S,4S,5R)-4-Methyl-5-phenyl-3-p-toluenesulfonyl-2-<(1S,2R)-1-hydroxy-2-carbomethoxy>propyloxazolidine

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Technology Process of (2S,4S,5R)-4-Methyl-5-phenyl-3-p-toluenesulfonyl-2-<(1S,2R)-1-hydroxy-2-carbomethoxy>propyloxazolidine

There total 2 articles about (2S,4S,5R)-4-Methyl-5-phenyl-3-p-toluenesulfonyl-2-<(1S,2R)-1-hydroxy-2-carbomethoxy>propyloxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119588-69-1
(2S,3S)-3-[(2S,4S,5R)-4-Methyl-5-phenyl-3-(toluene-4-sulfonyl)-oxazolidin-2-yl]-oxirane-2-carboxylic acid

: 129611-60-5
(2S,4S,5R)-4-Methyl-5-phenyl-3-p-toluenesulfonyl-2-<(1S,2R)-1-hydroxy-2-carbomethoxy>propyloxazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / tetrahydrofuran / 5 h / 0 °C

2: 1. methanolic KOH, 2. Bu₄NHSO₄ / Bu₄NHSO₄ / 1. 5 min; 2. CH₃CN, RT, overnight

With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; tetra(n-butyl)ammonium hydrogensulfate; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)89766-0

Reference yield:

: 128227-36-1,129705-13-1
(2S,4S,5R)-4-Methyl-5-phenyl-3-p-toluenesulfonyl-2-<(1S,2R)-1-hydroxy-2-carboxy>propyloxazolidine

: 74-88-4
methyl iodide

: 129611-60-5
(2S,4S,5R)-4-Methyl-5-phenyl-3-p-toluenesulfonyl-2-<(1S,2R)-1-hydroxy-2-carbomethoxy>propyloxazolidine

Guidance literature:: With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; tetra(n-butyl)ammonium hydrogensulfate; Yield given. Multistep reaction; 1. 5 min; 2. CH₃CN, RT, overnight;
DOI:10.1016/S0040-4020(01)89766-0