(4′-chlorobenzyl)-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-1-β-D-glucopyranoside

Base Information

Chemical Name:(4′-chlorobenzyl)-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-1-β-D-glucopyranoside
CAS No.:1239365-12-8
Molecular Formula:C₃₆H₃₈ClN₃O₆Si
Molecular Weight:672.253
Hs Code.:

Synonyms:(4′-chlorobenzyl)-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-1-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4′-chlorobenzyl)-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-1-β-D-glucopyranoside

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Technology Process of (4′-chlorobenzyl)-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-1-β-D-glucopyranoside

There total 2 articles about (4′-chlorobenzyl)-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-1-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 659722-21-1
methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside

: 873-76-7
para-Chlorobenzyl alcohol

: 1239365-10-6
(4′-chlorobenzyl)-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-1-α-D-glucopyranoside

: 1239365-12-8
(4′-chlorobenzyl)-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-1-β-D-glucopyranoside

Guidance literature:: methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside; para-Chlorobenzyl alcohol; In dichloromethane; at 20 ℃; for 1h; Molecular sieve; Inert atmosphere;

With dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; at 20 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1021/ci4000882

Reference yield:

: 1239364-99-8
bromo-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-D-glucopyranoside

: 873-76-7
para-Chlorobenzyl alcohol

: 1239365-10-6
(4′-chlorobenzyl)-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-1-α-D-glucopyranoside

: 1239365-12-8
(4′-chlorobenzyl)-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-1-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 2.5h; optical yield given as %de; Molecular sieve; Inert atmosphere; Darkness;
DOI:10.1021/jm1002777