bromo-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-D-glucopyranoside

Base Information

Chemical Name:bromo-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-D-glucopyranoside
CAS No.:1239364-99-8
Molecular Formula:C₂₉H₃₂BrN₃O₅Si
Molecular Weight:610.58
Hs Code.:

Synonyms:bromo-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bromo-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-D-glucopyranoside

Chemical Property:

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Technology Process of bromo-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-D-glucopyranoside

There total 1 articles about bromo-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 659722-21-1
methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside

: 1239364-99-8
bromo-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-D-glucopyranoside

Guidance literature:: With bromine; potassium carbonate; In dichloromethane; at 0 - 25 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1021/jm1002777

Reference yield:

: 1239364-99-8
bromo-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-D-glucopyranoside

: 873-76-7
para-Chlorobenzyl alcohol

: 1239365-10-6
(4′-chlorobenzyl)-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-1-α-D-glucopyranoside

: 1239365-12-8
(4′-chlorobenzyl)-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-1-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 2.5h; optical yield given as %de; Molecular sieve; Inert atmosphere; Darkness;
DOI:10.1021/jm1002777

Reference yield:

: 1239364-99-8
bromo-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-D-glucopyranoside

: 100-51-6,185532-71-2
benzyl alcohol

: benzyl 2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-α-D-glucopyranoside

: 1239365-01-5
benzyl 2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 2.5h; optical yield given as %de; Molecular sieve; Inert atmosphere; Darkness;
DOI:10.1021/jm1002777