methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside
CAS No.:659722-21-1
Molecular Formula:C₃₀H₃₅N₃O₅SSi
Molecular Weight:577.777
Hs Code.:

Synonyms:methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside

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Chemical Property of methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside

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Technology Process of methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside

There total 5 articles about methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.7%

: 501088-53-5
methyl 2-azido-3-O-benzoyl-2-deoxy-1-thio-β-D-glucopyranoside

: 58479-61-1
tert-butylchlorodiphenylsilane

: 659722-21-1
methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: With 1H-imidazole; In dichloromethane; for 2h; Inert atmosphere; Reflux;
DOI:10.1071/CH09480

Reference yield:

: 501089-55-0
C₂₃H₃₁N₃O₄SSi

: 98-88-4
benzoyl chloride

: 659722-21-1
methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside

: 659722-20-0
C₃₀H₃₅N₃O₅SSi

Guidance literature:: C₂₃H₃₁N₃O₄SSi; With di(n-butyl)tin oxide; In methanol;

benzoyl chloride; In methanol; at 20 ℃; for 24h;

Reference yield:

: 282526-04-9
methyl 2-azido-2-deoxy-1-thio-β-D-glucopyranoside

: 659722-21-1
methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / acetonitrile

2: dmap / 1,2-dichloro-ethane

3: methanol; toluene-4-sulfonic acid / acetonitrile

4: dmap / 1,2-dichloro-ethane

With methanol; dmap; toluene-4-sulfonic acid; In 1,2-dichloro-ethane; acetonitrile;