2,6-bis-trifluoromethylbenzoic acid 2-[1-(ethoxycarbonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

Base Information

Chemical Name:2,6-bis-trifluoromethylbenzoic acid 2-[1-(ethoxycarbonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester
CAS No.:1353091-91-4
Molecular Formula:C₂₃H₂₆F₆N₂O₆
Molecular Weight:540.46
Hs Code.:

Synonyms:2,6-bis-trifluoromethylbenzoic acid 2-[1-(ethoxycarbonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

Suppliers and Price of 2,6-bis-trifluoromethylbenzoic acid 2-[1-(ethoxycarbonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,6-bis-trifluoromethylbenzoic acid 2-[1-(ethoxycarbonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,6-bis-trifluoromethylbenzoic acid 2-[1-(ethoxycarbonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

There total 5 articles about 2,6-bis-trifluoromethylbenzoic acid 2-[1-(ethoxycarbonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1353048-81-3
[2-(2-bromomethylacryloylamino)-4-methylpentanoylamino]acetic acid ethyl ester

: 1353048-90-4
2,6-bis(trifluoromethyl)benzoic acid cesium salt

: 1353091-91-4
2,6-bis-trifluoromethylbenzoic acid 2-[1-(ethoxycarbonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

Guidance literature:: In acetone; Reflux;
DOI:10.1021/jm201359d

Reference yield:

: 2999-46-4
Ethyl isocyanoacetate

: 1353091-91-4
2,6-bis-trifluoromethylbenzoic acid 2-[1-(ethoxycarbonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 0.5 h

1.2: 6 h / 0 °C

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

3.1: acetone / Reflux

With trifluoroacetic acid; In ethanol; dichloromethane; acetone;
DOI:10.1021/jm201359d

Reference yield:

: 1353048-87-9
{2-[(2-bromomethylacryloyl)-(2,4-dimethoxybenzyl)amino]-4-ethylpentanoylamino}acetic acid ethyl ester

: 1353091-91-4
2,6-bis-trifluoromethylbenzoic acid 2-[1-(ethoxycarbonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2: acetone / Reflux

With trifluoroacetic acid; In dichloromethane; acetone;
DOI:10.1021/jm201359d