{2-[(2-bromomethylacryloyl)-(2,4-dimethoxybenzyl)amino]-4-ethylpentanoylamino}acetic acid ethyl ester

Base Information

Chemical Name:{2-[(2-bromomethylacryloyl)-(2,4-dimethoxybenzyl)amino]-4-ethylpentanoylamino}acetic acid ethyl ester
CAS No.:1353048-87-9
Molecular Formula:C₂₃H₃₃BrN₂O₆
Molecular Weight:513.429
Hs Code.:

Synonyms:{2-[(2-bromomethylacryloyl)-(2,4-dimethoxybenzyl)amino]-4-ethylpentanoylamino}acetic acid ethyl ester

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Chemical Property of {2-[(2-bromomethylacryloyl)-(2,4-dimethoxybenzyl)amino]-4-ethylpentanoylamino}acetic acid ethyl ester

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Technology Process of {2-[(2-bromomethylacryloyl)-(2,4-dimethoxybenzyl)amino]-4-ethylpentanoylamino}acetic acid ethyl ester

There total 1 articles about {2-[(2-bromomethylacryloyl)-(2,4-dimethoxybenzyl)amino]-4-ethylpentanoylamino}acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 2999-46-4
Ethyl isocyanoacetate

: 20781-20-8
2,4-Dimethoxybenzylamine

: 72707-66-5
2-(bromomethyl)acrylic acid

: 590-86-3
isovaleraldehyde

: 1353048-87-9
{2-[(2-bromomethylacryloyl)-(2,4-dimethoxybenzyl)amino]-4-ethylpentanoylamino}acetic acid ethyl ester

Guidance literature:: 2,4-Dimethoxybenzylamine; isovaleraldehyde; In ethanol; for 0.5h;

Ethyl isocyanoacetate; 2-(bromomethyl)acrylic acid; In ethanol; at 0 ℃; for 6h;
DOI:10.1021/jm201359d

Reference yield:

: 1353048-87-9
{2-[(2-bromomethylacryloyl)-(2,4-dimethoxybenzyl)amino]-4-ethylpentanoylamino}acetic acid ethyl ester

: 1353091-91-4
2,6-bis-trifluoromethylbenzoic acid 2-[1-(ethoxycarbonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2: acetone / Reflux

With trifluoroacetic acid; In dichloromethane; acetone;
DOI:10.1021/jm201359d

Reference yield:

: 1353048-87-9
{2-[(2-bromomethylacryloyl)-(2,4-dimethoxybenzyl)amino]-4-ethylpentanoylamino}acetic acid ethyl ester

: 1353048-83-5
2,6-dichlorobenzoic acid 2-[1-(ethoxycarbonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2: acetone / Reflux

With trifluoroacetic acid; In dichloromethane; acetone;
DOI:10.1021/jm201359d