C₃₂H₃₇N₃O₅

Base Information

Chemical Name:C₃₂H₃₇N₃O₅
CAS No.:1384107-23-6
Molecular Formula:C₃₂H₃₇N₃O₅
Molecular Weight:543.663
Hs Code.:

C<sub>32</sub>H<sub>37</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₃₂H₃₇N₃O₅

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Chemical Property of C₃₂H₃₇N₃O₅

Chemical Property:

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Technology Process of C₃₂H₃₇N₃O₅

There total 3 articles about C₃₂H₃₇N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 844856-99-1
2-benzyloxy-2-(8-benzyloxy-1,4-dioxaspiro[4.5]dec-7-yl)-1-(4-methoxybenzyl)ethylamine

: 1384107-23-6
C₃₂H₃₇N₃O₅

Guidance literature:: With imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate; In methanol; at 0 ℃; for 24h;
DOI:10.1021/ol301331t

Reference yield:

: 844856-96-8
[2-hydroxy-2-(8-hydroxy-1,4-dioxaspiro[4.5]dec-7-yl)-1-(4-methoxybenzyl)ethyl]carbamic acid tert-butyl ester

: 1384107-23-6
C₃₂H₃₇N₃O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 - 20 °C / Cooling with ice

2.1: 2,6-dimethylpyridine; t-butyldimethylsiyl triflate / dichloromethane / 1 h / 0 °C

2.2: 0 °C

3.1: imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate / methanol / 24 h / 0 °C

With 2,6-dimethylpyridine; imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; t-butyldimethylsiyl triflate; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; In methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol301331t

Reference yield:

: 100-39-0
benzyl bromide

: 1384107-23-6
C₃₂H₃₇N₃O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 - 20 °C / Cooling with ice

2.1: 2,6-dimethylpyridine; t-butyldimethylsiyl triflate / dichloromethane / 1 h / 0 °C

2.2: 0 °C

3.1: imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate / methanol / 24 h / 0 °C

With 2,6-dimethylpyridine; imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; t-butyldimethylsiyl triflate; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; In methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol301331t