2-(1-methoxy-2-(trimethylsilyl)ethyl)-4,4-dimethylcyclohexane-1-carboxaldehyde dimethyl acetal

Base Information

Chemical Name:2-(1-methoxy-2-(trimethylsilyl)ethyl)-4,4-dimethylcyclohexane-1-carboxaldehyde dimethyl acetal
CAS No.:134923-05-0
Molecular Formula:C₁₇H₃₆O₃Si
Molecular Weight:316.557
Hs Code.:

Synonyms:2-(1-methoxy-2-(trimethylsilyl)ethyl)-4,4-dimethylcyclohexane-1-carboxaldehyde dimethyl acetal

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Chemical Property of 2-(1-methoxy-2-(trimethylsilyl)ethyl)-4,4-dimethylcyclohexane-1-carboxaldehyde dimethyl acetal

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Technology Process of 2-(1-methoxy-2-(trimethylsilyl)ethyl)-4,4-dimethylcyclohexane-1-carboxaldehyde dimethyl acetal

There total 6 articles about 2-(1-methoxy-2-(trimethylsilyl)ethyl)-4,4-dimethylcyclohexane-1-carboxaldehyde dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 67-56-1
methanol

: 134922-94-4
5,5-dimethyl-1-methoxy-9-(trimethylsilyl)-(E,Z)-1,7-nonadiene

: 134923-03-8,134923-04-9,136067-03-3,136067-04-4
2-ethenyl-4,4-dimethylcyclohexane-1-carboxaldehyde dimethyl acetal

: 134923-05-0
2-(1-methoxy-2-(trimethylsilyl)ethyl)-4,4-dimethylcyclohexane-1-carboxaldehyde dimethyl acetal

Guidance literature:: With 2,6-dimethylpyridine; lithium perchlorate; In dichloromethane; electrolysis (carbon electrodes, const. current);
DOI:10.1021/ja00019a038

Reference yield: 13.0%

: 134922-94-4,136066-95-0,136066-96-1,136066-97-2,136066-98-3
((2E,8Z)-9-Methoxy-5,5-dimethyl-nona-2,8-dienyl)-trimethyl-silane

: 134923-03-8,134923-04-9,136067-03-3,136067-04-4
2-ethenyl-4,4-dimethylcyclohexane-1-carboxaldehyde dimethyl acetal

: 134923-05-0
2-(1-methoxy-2-(trimethylsilyl)ethyl)-4,4-dimethylcyclohexane-1-carboxaldehyde dimethyl acetal

Guidance literature:: In methanol; dichloromethane; anodic oxidation (reticulated vitreous carbon anode);
DOI:10.1016/S0040-4039(00)79910-2

Reference yield:

: (E)-4,4-Dimethyl-8-trimethylsilanyl-oct-6-enal

: 134923-05-0
2-(1-methoxy-2-(trimethylsilyl)ethyl)-4,4-dimethylcyclohexane-1-carboxaldehyde dimethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, hexane, RT, 1 h, 2.) THF, hexane, RT, 16 h

2: 13 percent / 2,6-lutidine, LiClO₄ / CH₂Cl₂ / electrolysis (carbon electrodes, const. current)

With 2,6-dimethylpyridine; n-butyllithium; lithium perchlorate; In dichloromethane;
DOI:10.1021/ja00019a038