diethyl 1-(4-methoxyphenyl)-4-((4-methoxyphenyl)amino)-5-oxo-2,5-dihydro-1H-pyrrole-2,3-dicarboxylate

Base Information

Chemical Name:diethyl 1-(4-methoxyphenyl)-4-((4-methoxyphenyl)amino)-5-oxo-2,5-dihydro-1H-pyrrole-2,3-dicarboxylate
CAS No.:1404481-52-2
Molecular Formula:C₂₄H₂₆N₂O₇
Molecular Weight:454.48
Hs Code.:

Synonyms:diethyl 1-(4-methoxyphenyl)-4-((4-methoxyphenyl)amino)-5-oxo-2,5-dihydro-1H-pyrrole-2,3-dicarboxylate

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Chemical Property of diethyl 1-(4-methoxyphenyl)-4-((4-methoxyphenyl)amino)-5-oxo-2,5-dihydro-1H-pyrrole-2,3-dicarboxylate

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Technology Process of diethyl 1-(4-methoxyphenyl)-4-((4-methoxyphenyl)amino)-5-oxo-2,5-dihydro-1H-pyrrole-2,3-dicarboxylate

There total 4 articles about diethyl 1-(4-methoxyphenyl)-4-((4-methoxyphenyl)amino)-5-oxo-2,5-dihydro-1H-pyrrole-2,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 924-44-7
glyoxylic acid ethyl ester

: 104-94-9
4-methoxy-aniline

: 762-21-0
acetylenedicarboxylic acid diethyl ester

: 1404481-52-2
diethyl 1-(4-methoxyphenyl)-4-((4-methoxyphenyl)amino)-5-oxo-2,5-dihydro-1H-pyrrole-2,3-dicarboxylate

Guidance literature:: 4-methoxy-aniline; acetylenedicarboxylic acid diethyl ester; In ethanol; at 20 ℃; for 0.166667h;

glyoxylic acid ethyl ester; With benzoic acid; In ethanol; toluene; at 20 ℃; for 48h;
DOI:10.1016/j.tet.2012.11.018

Reference yield: 68.0%

: 924-44-7
glyoxylic acid ethyl ester

: 104-94-9
4-methoxy-aniline

: 1404481-52-2
diethyl 1-(4-methoxyphenyl)-4-((4-methoxyphenyl)amino)-5-oxo-2,5-dihydro-1H-pyrrole-2,3-dicarboxylate

Guidance literature:: With palladium(II) trifluoroacetate; sodium sulfate; In toluene; at 70 ℃; for 48h; Temperature; Solvent; Concentration; Reagent/catalyst; Inert atmosphere; Sealed tube;
DOI:10.1021/ol302483f

Reference yield: 9.0%

: 924-44-7
glyoxylic acid ethyl ester

: 106-47-8
4-chloro-aniline

: 104-94-9
4-methoxy-aniline

: 1404481-52-2
diethyl 1-(4-methoxyphenyl)-4-((4-methoxyphenyl)amino)-5-oxo-2,5-dihydro-1H-pyrrole-2,3-dicarboxylate

: 1404481-60-2
diethyl 1-(4-chlorophenyl)-4-((4-chlorophenyl)amino)-5-oxo-2,5-dihydro-1H-pyrrole-2,3-dicarboxylate

: 1404481-71-5
diethyl 1-(4-chlorophenyl)-4-((4-methoxyphenyl)amino)-5-oxo-2,5-dihydro-1H-pyrrole-2,3-dicarboxylate

: 1404481-72-6
diethyl 4-((4-chlorophenyl)amino)-1-(4-methoxyphenyl)-5-oxo-2,5-dihydro-1H-pyrrole-2,3-dicarboxylate

Guidance literature:: With palladium(II) trifluoroacetate; sodium sulfate; In toluene; at 70 ℃; for 24h; Inert atmosphere; Sealed tube;
DOI:10.1021/ol302483f