N^ω-benzyloxycarbonyl-N^α-tert-butyloxycarbonyl-N^ω'-methoxy-L-arginine tert-butyl ester

Base Information

• Chemical Name: N^ω-benzyloxycarbonyl-N^α-tert-butyloxycarbonyl-N^ω'-methoxy-L-arginine tert-butyl ester
• CAS No.: 1061261-93-5
• Molecular Formula: C₂₄H₃₈N₄O₇
• Molecular Weight: 494.588

Synonyms:N^ω-benzyloxycarbonyl-N^α-tert-butyloxycarbonyl-N^ω'-methoxy-L-arginine tert-butyl ester

Chemical Property of N^ω-benzyloxycarbonyl-N^α-tert-butyloxycarbonyl-N^ω'-methoxy-L-arginine tert-butyl ester

Chemical Property:

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Technology Process of N^ω-benzyloxycarbonyl-N^α-tert-butyloxycarbonyl-N^ω'-methoxy-L-arginine tert-butyl ester

There total 4 articles about N^ω-benzyloxycarbonyl-N^α-tert-butyloxycarbonyl-N^ω'-methoxy-L-arginine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Nω-benzyloxycarbonyl-Nα-tert-butyloxycarbonyl-L-thiocitrulline tert-butyl ester (1061261-89-9) + N-methoxylamine hydrochloride (593-56-6) → Nω-benzyloxycarbonyl-Nα-tert-butyloxycarbonyl-Nω'-methoxy-L-arginine t-butyl ester (1061261-93-5)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

DOI:10.1039/c0ob01117g

Reference yield: 95.0%

Nω-benzyloxycarbonyl-Nα-tert-butyloxycarbonyl-L-thiocitrulline tert-butyl ester (1061261-89-9) + N-methoxylamine hydrochloride (593-56-6) → Nω-benzyloxycarbonyl-Nα-tert-butyloxycarbonyl-Nω'-methoxy-L-arginine tert-butyl ester (1061261-93-5)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;

DOI:10.1055/s-2008-1067165

Reference yield:

benzyloxycarbonyl isothiocyanate (63220-36-0) → Nω-benzyloxycarbonyl-Nα-tert-butyloxycarbonyl-Nω'-methoxy-L-arginine t-butyl ester (1061261-93-5)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane / 2.5 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;

DOI:10.1039/c0ob01117g

upstream raw materials:

N^ω-benzyloxycarbonyl-N^α-tert-butyloxycarbonyl-L-thiocitrulline tert-butyl ester

N-methoxylamine hydrochloride

benzyloxycarbonyl isothiocyanate

tert-butyl (2S)-5-amino-2-[(2-methylpropan-2-yl)oxycarbonylamino]pentanoate

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