N-Cyanmethyl-3-nitranilin

Base Information

• Chemical Name: N-Cyanmethyl-3-nitranilin
• CAS No.: 4718-05-2
• Molecular Formula: C₈H₇N₃O₂
• Molecular Weight: 177.162

Synonyms:N-Cyanmethyl-3-nitranilin

Chemical Property of N-Cyanmethyl-3-nitranilin

Chemical Property:

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Technology Process of N-Cyanmethyl-3-nitranilin

There total 2 articles about N-Cyanmethyl-3-nitranilin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

3-nitro-aniline (99-09-2) + acetonitrile (75-05-8,26809-02-9) → N-Cyanmethyl-3-nitranilin (4718-05-2)

Guidance literature:

With potassium carbonate; potassium iodide; at 100 ℃; for 48h;

DOI:10.1016/j.bioorg.2019.102994

Reference yield:

→ N-Cyanmethyl-3-nitranilin (4718-05-2)

Guidance literature:

m-O2N-C6H4-NH2, Paraform, KCN + (wenig) ZnCl2 in Eg. <50grad, 8h>;

Reference yield:

oxalyl dichloride (79-37-8) + N-Cyanmethyl-3-nitranilin (4718-05-2) → C10H5Cl2N3O3

Guidance literature:

With triethylamine hydrochloride; In toluene; for 0.75h;

DOI:10.1016/j.bioorg.2019.102994

upstream raw materials:

3-nitro-aniline

acetonitrile

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