S-[2-(N-methyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

Base Information

Chemical Name:S-[2-(N-methyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate
CAS No.:352556-35-5
Molecular Formula:C₂₀H₂₂N₂OS
Molecular Weight:338.473
Hs Code.:

Synonyms:S-[2-(N-methyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-[2-(N-methyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

Chemical Property:

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Technology Process of S-[2-(N-methyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

There total 5 articles about S-[2-(N-methyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 352556-29-7
S-[2-(N-3'-p-tolylprop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

: 74-88-4
methyl iodide

: 352556-35-5
S-[2-(N-methyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

Guidance literature:: With potassium carbonate; In acetone; for 10h; Heating;
DOI:10.1021/jo001783+

Reference yield:

: 13511-84-7
S-(2-nitrophenyl)-N,N-dimethylcarbamothioate

: 352556-35-5
S-[2-(N-methyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 89 percent / Fe; water; glacial acetic acid / 8 h / 20 °C

2.1: K₂CO₃ / acetone / 5 h / 20 °C

2.2: 84 percent / acetone / 16 h / Heating

3.1: 92 percent / CuI; Et₃N / PdCl₂(PPh₃)2 / acetonitrile / 24 h / 20 °C

4.1: 96 percent / K₂CO₃ / acetone / 10 h / Heating

With copper(l) iodide; water; iron; potassium carbonate; acetic acid; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In acetone; acetonitrile;
DOI:10.1021/jo001783+

Reference yield:

: 624-31-7
4-tolyl iodide

: 352556-35-5
S-[2-(N-methyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CuI; Et₃N / PdCl₂(PPh₃)2 / acetonitrile / 24 h / 20 °C

2: 96 percent / K₂CO₃ / acetone / 10 h / Heating

With copper(l) iodide; potassium carbonate; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In acetone; acetonitrile;
DOI:10.1021/jo001783+