4-((tert-butyldimethylsilanyl)oxymethyl)-6-iodo-2,3-dimethoxybenzoic acid methyl ester

Base Information

Chemical Name:4-((tert-butyldimethylsilanyl)oxymethyl)-6-iodo-2,3-dimethoxybenzoic acid methyl ester
CAS No.:350245-33-9
Molecular Formula:C₁₇H₂₇IO₅Si
Molecular Weight:466.388
Hs Code.:

Synonyms:4-((tert-butyldimethylsilanyl)oxymethyl)-6-iodo-2,3-dimethoxybenzoic acid methyl ester

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Chemical Property of 4-((tert-butyldimethylsilanyl)oxymethyl)-6-iodo-2,3-dimethoxybenzoic acid methyl ester

Chemical Property:

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Technology Process of 4-((tert-butyldimethylsilanyl)oxymethyl)-6-iodo-2,3-dimethoxybenzoic acid methyl ester

There total 10 articles about 4-((tert-butyldimethylsilanyl)oxymethyl)-6-iodo-2,3-dimethoxybenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7168-94-7
dimethyl 2,3-dimethoxyterephthalate

: 350245-33-9
4-((tert-butyldimethylsilanyl)oxymethyl)-6-iodo-2,3-dimethoxybenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: AgNO₃; TFAA

2: H₂ / Raney Ni

3: H(+); NaNO₂; KI

4: LiOH / tetrahydrofuran; H₂O

5: BH₃ / tetrahydrofuran

6: imidazole

With 1H-imidazole; lithium hydroxide; borane; hydrogen; hydrogen cation; silver nitrate; trifluoroacetic anhydride; potassium iodide; sodium nitrite; nickel; In tetrahydrofuran; water; 1: Crivello method / 3: Sandmeyer reaction;
DOI:10.1016/S0040-4039(01)00524-X

Reference yield:

: 75956-62-6
dimethyl 2,3-dihydroxyterephthalate

: 350245-33-9
4-((tert-butyldimethylsilanyl)oxymethyl)-6-iodo-2,3-dimethoxybenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 100 percent / K₂CO₃

2: AgNO₃; TFAA

3: H₂ / Raney Ni

4: H(+); NaNO₂; KI

5: LiOH / tetrahydrofuran; H₂O

6: BH₃ / tetrahydrofuran

7: imidazole

With 1H-imidazole; lithium hydroxide; borane; hydrogen; hydrogen cation; potassium carbonate; silver nitrate; trifluoroacetic anhydride; potassium iodide; sodium nitrite; nickel; In tetrahydrofuran; water; 2: Crivello method / 4: Sandmeyer reaction;
DOI:10.1016/S0040-4039(01)00524-X

Reference yield:

: 19829-72-2
2,3-dihydroxyterephthalic acid

: 350245-33-9
4-((tert-butyldimethylsilanyl)oxymethyl)-6-iodo-2,3-dimethoxybenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 75 percent / HCl

2: 100 percent / K₂CO₃

3: AgNO₃; TFAA

4: H₂ / Raney Ni

5: H(+); NaNO₂; KI

6: LiOH / tetrahydrofuran; H₂O

7: BH₃ / tetrahydrofuran

8: imidazole

With 1H-imidazole; hydrogenchloride; lithium hydroxide; borane; hydrogen; hydrogen cation; potassium carbonate; silver nitrate; trifluoroacetic anhydride; potassium iodide; sodium nitrite; nickel; In tetrahydrofuran; water; 1: Fischer esterification / 3: Crivello method / 5: Sandmeyer reaction;
DOI:10.1016/S0040-4039(01)00524-X