2-<(benzyloxycarbonyl)(3,4-dimethoxyphenethyl)amino>-1-(4-benzyloxyphenyl)ethanone

Base Information

Chemical Name:2-<(benzyloxycarbonyl)(3,4-dimethoxyphenethyl)amino>-1-(4-benzyloxyphenyl)ethanone
CAS No.:71709-05-2
Molecular Formula:C₃₃H₃₃NO₆
Molecular Weight:539.628
Hs Code.:

Synonyms:2-<(benzyloxycarbonyl)(3,4-dimethoxyphenethyl)amino>-1-(4-benzyloxyphenyl)ethanone

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Chemical Property of 2-<(benzyloxycarbonyl)(3,4-dimethoxyphenethyl)amino>-1-(4-benzyloxyphenyl)ethanone

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Technology Process of 2-<(benzyloxycarbonyl)(3,4-dimethoxyphenethyl)amino>-1-(4-benzyloxyphenyl)ethanone

There total 1 articles about 2-<(benzyloxycarbonyl)(3,4-dimethoxyphenethyl)amino>-1-(4-benzyloxyphenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.1%

: 501-53-1,94274-21-2
benzyl chloroformate

: 2-(3,4-dimethoxyphenethyl)amino-1-(4-benzyloxyphenyl)ethanone hydrochloride

: 71709-05-2
2-<(benzyloxycarbonyl)(3,4-dimethoxyphenethyl)amino>-1-(4-benzyloxyphenyl)ethanone

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 0 - 20 ℃; for 1.33333h;
DOI:10.1248/cpb.41.639

Reference yield: 96.0%

: 71709-05-2
2-<(benzyloxycarbonyl)(3,4-dimethoxyphenethyl)amino>-1-(4-benzyloxyphenyl)ethanone

: 151323-98-7
[(R)-2-(4-Benzyloxy-phenyl)-2-hydroxy-ethyl]-[2-(3,4-dimethoxy-phenyl)-ethyl]-carbamic acid benzyl ester

Guidance literature:: With borane-1,4-oxathiane; (R)-(+)-2-amino-3-methyl-1,1-diphenylbutan-1-ol; In tetrahydrofuran; at 3 - 5 ℃; for 1h;
DOI:10.1248/cpb.41.639

Reference yield:

: 71709-05-2
2-<(benzyloxycarbonyl)(3,4-dimethoxyphenethyl)amino>-1-(4-benzyloxyphenyl)ethanone

: 71771-90-9
denopamine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / borane-oxathiane, (R)-(+)-2-amino-3-methyl-1,1-diphenylbutan-1-ol / tetrahydrofuran / 1 h / 3 - 5 °C

2: 69 percent / H₂ / 10percent Pd/C / methanol / 760 Torr / Ambient temperature

With borane-1,4-oxathiane; hydrogen; (R)-(+)-2-amino-3-methyl-1,1-diphenylbutan-1-ol; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1248/cpb.41.639