3-<4-(3-chlorophenyl)-1-piperazinyl>-3-methylbutanoic acid ethyl ester

Base Information

Chemical Name:3-<4-(3-chlorophenyl)-1-piperazinyl>-3-methylbutanoic acid ethyl ester
CAS No.:220910-01-0
Molecular Formula:C₁₆H₂₃ClN₂O₂
Molecular Weight:310.824
Hs Code.:

Synonyms:3-<4-(3-chlorophenyl)-1-piperazinyl>-3-methylbutanoic acid ethyl ester

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Chemical Property of 3-<4-(3-chlorophenyl)-1-piperazinyl>-3-methylbutanoic acid ethyl ester

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Technology Process of 3-<4-(3-chlorophenyl)-1-piperazinyl>-3-methylbutanoic acid ethyl ester

There total 1 articles about 3-<4-(3-chlorophenyl)-1-piperazinyl>-3-methylbutanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 10544-63-5
ethyl crotonate

: 6640-24-0
N-(m-chlorophenyl)piperazine

: 220910-01-0
3-<4-(3-chlorophenyl)-1-piperazinyl>-3-methylbutanoic acid ethyl ester

Guidance literature:: With sodium ethanolate; In ethanol; at 60 ℃; for 2h;
DOI:10.1021/jm970700n

Reference yield: 95.0%

: 220910-01-0
3-<4-(3-chlorophenyl)-1-piperazinyl>-3-methylbutanoic acid ethyl ester

: 220910-02-1
4-(3-chlorophenyl)-1-(3-hydroxy-1-methylpropyl)piperazine

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In diethyl ether; toluene; for 2h; Ambient temperature;
DOI:10.1021/jm970700n

Reference yield:

: 220910-01-0
3-<4-(3-chlorophenyl)-1-piperazinyl>-3-methylbutanoic acid ethyl ester

: 151447-89-1
4-(3-chlorophenyl)-1-(3-chloro-1-methylpropyl)piperazine

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / sodium bis(2-methoxyethoxy)aluminum hydride / diethyl ether; toluene / 2 h / Ambient temperature

2: 82 percent / SOCl₂ / CHCl₃ / 1 h / Heating

With thionyl chloride; sodium bis(2-methoxyethoxy)aluminium dihydride; In diethyl ether; chloroform; toluene;
DOI:10.1021/jm970700n