C₉H₉ClO₂Zn

Base Information

Chemical Name:C₉H₉ClO₂Zn
CAS No.:1072906-23-0
Molecular Formula:C₉H₉ClO₂Zn
Molecular Weight:250.012
Hs Code.:

C<sub>9</sub>H<sub>9</sub>ClO<sub>2</sub>Zn

Synonyms:C₉H₉ClO₂Zn

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Chemical Property of C₉H₉ClO₂Zn

Chemical Property:

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Technology Process of C₉H₉ClO₂Zn

There total 1 articles about C₉H₉ClO₂Zn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58313-23-8
3-iodobenzoic acid methyl ester

: 7646-85-7,24359-56-6
zinc(II) chloride

: 1072906-23-0
C₉H₉ClO₂Zn

Guidance literature:: 3-iodobenzoic acid methyl ester; With TurboGrignard; In tetrahydrofuran; at -20 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

zinc(II) chloride; In tetrahydrofuran; at -20 - 20 ℃; for 0.25h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.9b04564

Reference yield: 96.0%

: 1072906-23-0
C₉H₉ClO₂Zn

: 98-88-4
benzoyl chloride

: 130339-72-9
Ethyl m-benzoylbenzoate

Guidance literature:: ((t-Bu)2POH)2PdCl₂; In 1-methyl-pyrrolidin-2-one; at 25 ℃; for 0.5h;
DOI:10.1021/jo801445y

Reference yield: 52.0%

: 1072906-23-0
C₉H₉ClO₂Zn

: (2R,5R,6R)-5-bromo-2-(tert-butyl)-6-methyl-1,3-dioxan-4-one

: ethyl 3-((2R,4R,5R)-2-(tert-butyl)-4-methyl-6-oxo-1,3-dioxan-5-yl)benzoate

Guidance literature:: With triphenylphosphine; cobalt(II) chloride; In tetrahydrofuran; at -20 - 25 ℃; for 16h; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.9b04564