C₁₄H₂₀O

Base Information

• Chemical Name: C₁₄H₂₀O
• CAS No.: 1206489-19-1
• Molecular Formula: C₁₄H₂₀O
• Molecular Weight: 204.312
• Mol file: 1206489-19-1.mol

Synonyms:C₁₄H₂₀O

Chemical Property of C₁₄H₂₀O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₀O

There total 6 articles about C₁₄H₂₀O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

C15H22OSi (1338001-20-9) + methyl iodide (74-88-4) → C14H20O (1206489-19-1)

Guidance literature:

C₁₅H₂₂OSi; With methyllithium; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.5h; Inert atmosphere;

With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; In tetrahydrofuran; diethyl ether; at 20 ℃; for 0.5h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; diethyl ether; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1002/anie.201103886

Reference yield:

2-phenyl-3-octene-2-ol (821017-71-4) → C14H20O (1206489-19-1)

Guidance literature:

With salicylic acid; In water; acetonitrile; at 80 ℃; for 10h;

DOI:10.1021/ol500456s

Reference yield:

2-phenyloct-3-yn-2-ol (18215-71-9) → C14H20O (1206489-19-1)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride; sodium methylate / tetrahydrofuran / 1.5 h / 60 °C

2: salicylic acid / water; acetonitrile / 10 h / 80 °C

With lithium aluminium tetrahydride; sodium methylate; salicylic acid; In tetrahydrofuran; water; acetonitrile;

DOI:10.1021/ol500456s

upstream raw materials:

C₁₅H₂₂OSi

methyl iodide

pentanal

1-phenylhept-1-yn-3-ol

Downstream raw materials:

(E)-2-phenyloct-2-en-4-yl acetate:

(Z)-2-phenyloct-2-en-4-yl acetate:

(E)-(4-methyldeca-1,5-dien-4-yl)benzene