N,N',N''-(2,2',2''-(2,2',2''-(2,2',2''-(benzene-1,3,5-triyltris(oxy))tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(4-azido-2,3,5,6-tetrafluorobenzamide)

Base Information

Chemical Name:N,N',N''-(2,2',2''-(2,2',2''-(2,2',2''-(benzene-1,3,5-triyltris(oxy))tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(4-azido-2,3,5,6-tetrafluorobenzamide)
CAS No.:1400565-38-9
Molecular Formula:C₄₅H₄₂F₁₂N₁₂O₁₂
Molecular Weight:1170.88
Hs Code.:

N,N',N''-(2,2',2''-(2,2',2''-(2,2',2''-(benzene-1,3,5-triyltris(oxy))tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(4-azido-2,3,5,6-tetrafluorobenzamide)

Synonyms:N,N',N''-(2,2',2''-(2,2',2''-(2,2',2''-(benzene-1,3,5-triyltris(oxy))tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(4-azido-2,3,5,6-tetrafluorobenzamide)

Suppliers and Price of N,N',N''-(2,2',2''-(2,2',2''-(2,2',2''-(benzene-1,3,5-triyltris(oxy))tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(4-azido-2,3,5,6-tetrafluorobenzamide)

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Chemical Property of N,N',N''-(2,2',2''-(2,2',2''-(2,2',2''-(benzene-1,3,5-triyltris(oxy))tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(4-azido-2,3,5,6-tetrafluorobenzamide)

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Technology Process of N,N',N''-(2,2',2''-(2,2',2''-(2,2',2''-(benzene-1,3,5-triyltris(oxy))tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(4-azido-2,3,5,6-tetrafluorobenzamide)

There total 7 articles about N,N',N''-(2,2',2''-(2,2',2''-(2,2',2''-(benzene-1,3,5-triyltris(oxy))tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(4-azido-2,3,5,6-tetrafluorobenzamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 2,2',2''-(2,2',2''-(2,2',2''-(benzene-1,3,5-triyltris(oxy))tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(oxy)triethanaminium tris(2,2,2-trifluoroacetate)

: 126695-58-7
succinimidyl 4-azido-2,3,5,6-tetrafluorobenzoate

: 1400565-38-9
N,N',N''-(2,2',2''-(2,2',2''-(2,2',2''-(benzene-1,3,5-triyltris(oxy))tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(4-azido-2,3,5,6-tetrafluorobenzamide)

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1055/s-0031-1290444

Reference yield:

: 36629-42-2
methyl pentafluorobenzoate

: 1400565-38-9
N,N',N''-(2,2',2''-(2,2',2''-(2,2',2''-(benzene-1,3,5-triyltris(oxy))tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(4-azido-2,3,5,6-tetrafluorobenzamide)

Guidance literature:: Multi-step reaction with 4 steps

1: sodium azide / water; acetone / 8 h / Reflux

2: sodium hydroxide / methanol; water / 20 °C

3: dicyclohexyl-carbodiimide / dichloromethane / 20 °C

4: triethylamine / dichloromethane

With sodium azide; triethylamine; dicyclohexyl-carbodiimide; sodium hydroxide; In methanol; dichloromethane; water; acetone;
DOI:10.1055/s-0031-1290444

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 1400565-38-9
N,N',N''-(2,2',2''-(2,2',2''-(2,2',2''-(benzene-1,3,5-triyltris(oxy))tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(oxy)tris(ethane-2,1-diyl))tris(4-azido-2,3,5,6-tetrafluorobenzamide)

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran

2: dichloromethane / 1 h / 20 °C

3: triethylamine / dichloromethane

With triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 1: Mitsunobu reaction;
DOI:10.1055/s-0031-1290444