4-(4-hydroxy-2-oxo-2,5,6,7-tetrahydro-cyclopenta[b]pyran-3-yl)-butyric acid

Base Information

• Chemical Name: 4-(4-hydroxy-2-oxo-2,5,6,7-tetrahydro-cyclopenta[b]pyran-3-yl)-butyric acid
• CAS No.: 92848-16-3
• Molecular Formula: C₁₂H₁₄O₅
• Molecular Weight: 238.24

Synonyms:4-(4-hydroxy-2-oxo-2,5,6,7-tetrahydro-cyclopenta[b]pyran-3-yl)-butyric acid

Chemical Property of 4-(4-hydroxy-2-oxo-2,5,6,7-tetrahydro-cyclopenta[b]pyran-3-yl)-butyric acid

Chemical Property:

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Technology Process of 4-(4-hydroxy-2-oxo-2,5,6,7-tetrahydro-cyclopenta[b]pyran-3-yl)-butyric acid

There total 3 articles about 4-(4-hydroxy-2-oxo-2,5,6,7-tetrahydro-cyclopenta[b]pyran-3-yl)-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4,5,8,9,10-hexahydro-cyclopenta[5,6]pyrano[4,3-b]oxepin-2,6-dione (7257-02-5) → 1,5-pentanedioic acid (110-94-1) + 4-(4-hydroxy-2-oxo-2,5,6,7-tetrahydro-cyclopenta[b]pyran-3-yl)-butyric acid (92848-16-3)

Guidance literature:

With alkaline solution; dihydrogen peroxide;

DOI:10.1021/jo01046a042

Reference yield:

1-methyl-4-nitrosobenzene (623-11-0) + 3,4,5,8,9,10-hexahydro-cyclopenta[5,6]pyrano[4,3-b]oxepin-2,6-dione (7257-02-5) → 1,5-pentanedioic acid (110-94-1) + 4-(4-hydroxy-2-oxo-2,5,6,7-tetrahydro-cyclopenta[b]pyran-3-yl)-butyric acid (92848-16-3)

Guidance literature:

DOI:10.1021/jo01046a042

Reference yield:

3,4,5,8,9,10-hexahydro-cyclopenta[5,6]pyrano[4,3-b]oxepin-2,6-dione (7257-02-5) + dihydrogen peroxide (7722-84-1) → 1,5-pentanedioic acid (110-94-1) + 4-(4-hydroxy-2-oxo-2,5,6,7-tetrahydro-cyclopenta[b]pyran-3-yl)-butyric acid (92848-16-3)

Guidance literature:

DOI:10.1021/jo01046a042

upstream raw materials:

1-methyl-4-nitrosobenzene

3,4,5,8,9,10-hexahydro-cyclopenta[5,6]pyrano[4,3-b]oxepin-2,6-dione

dihydrogen peroxide

Downstream raw materials:

6-oxo-undecanedioic acid

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