C₁₇H₁₄N₄O₂S₂

Base Information

• Chemical Name: C₁₇H₁₄N₄O₂S₂
• CAS No.: 1438847-45-0
• Molecular Formula: C₁₇H₁₄N₄O₂S₂
• Molecular Weight: 370.456
• Mol file: 1438847-45-0.mol

Synonyms:C₁₇H₁₄N₄O₂S₂

Chemical Property of C₁₇H₁₄N₄O₂S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₄N₄O₂S₂

There total 4 articles about C₁₇H₁₄N₄O₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

C17H13N3O4S3 (1438847-42-7) + methylamine (74-89-5) → C17H14N4O2S2 (1438847-45-0)

Guidance literature:

In N,N-dimethyl-formamide; at 70 ℃; for 24h; Sealed tube;

DOI:10.1016/j.bmcl.2013.04.055

Reference yield:

C9H7N3S3 (397290-24-3) → C17H14N4O2S2 (1438847-45-0)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine; N-ethyl-N,N-diisopropylamine / 72 h / 0 - 20 °C

2: potassium permanganate; acetic acid / 1,4-dioxane; water / 24 h / 55 °C

3: N,N-dimethyl-formamide / 24 h / 70 °C / Sealed tube

With pyridine; potassium permanganate; acetic acid; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2013.04.055

Reference yield:

C17H13N3O2S3 (361173-08-2) → C17H14N4O2S2 (1438847-45-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium permanganate; acetic acid / 1,4-dioxane; water / 24 h / 55 °C

2: N,N-dimethyl-formamide / 24 h / 70 °C / Sealed tube

With potassium permanganate; acetic acid; In 1,4-dioxane; water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2013.04.055

upstream raw materials:

C₁₇H₁₃N₃O₂S₃

C₉H₇N₃S₃

C₁₇H₁₃N₃O₄S₃

methylamine