4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α-androst-9-en-3β-yl benzoate

Base Information

Chemical Name:4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α-androst-9-en-3β-yl benzoate
CAS No.:200120-83-8
Molecular Formula:C₂₆H₃₂O₄
Molecular Weight:408.538
Hs Code.:

Synonyms:4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α-androst-9-en-3β-yl benzoate

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Chemical Property of 4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α-androst-9-en-3β-yl benzoate

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Technology Process of 4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α-androst-9-en-3β-yl benzoate

There total 1 articles about 4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α-androst-9-en-3β-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 135573-96-5
3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-methanesulfonate

: 200120-83-8
4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α-androst-9-en-3β-yl benzoate

: C₂₆H₃₀O₃

Guidance literature:: With potassium acetate; In acetone; for 5h; Heating;
DOI:10.1135/cccc19971631

Reference yield: 63.0%

: 200120-83-8
4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α-androst-9-en-3β-yl benzoate

: C₂₆H₄₂O₃

: 200120-84-9
4aα,17β-Dihydroxy-4aβ-methyl-4a-homo-7,19-dinor-5α,9β,10β-androstan-3β-yl cyclohexanecarboxylate

Guidance literature:: With hydrogen; platinum; In acetic acid; for 24h; Ambient temperature;
DOI:10.1135/cccc19971631

Reference yield:

: 200120-83-8
4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α-androst-9-en-3β-yl benzoate

: C₂₇H₄₄O₄

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / H₂ / Pt / acetic acid / 24 h / Ambient temperature

2: 69 percent / Jones reagent / acetone / 0.17 h / 0 °C

3: 1.) Mg / 1.) ether, 2.) benzene, reflux, 3 h

With jones reagent; hydrogen; magnesium; platinum; In acetic acid; acetone;
DOI:10.1135/cccc19971631