3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-methanesulfonate

Base Information

Chemical Name:3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-methanesulfonate
CAS No.:135573-96-5
Molecular Formula:C₂₇H₃₄O₆S
Molecular Weight:486.629
Hs Code.:

Synonyms:3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-methanesulfonate

Chemical Property:

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Technology Process of 3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-methanesulfonate

There total 5 articles about 3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 135573-95-4
3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate

: 124-63-0
methanesulfonyl chloride

: 135573-96-5
3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-methanesulfonate

Guidance literature:: With pyridine; at 0 ℃; for 1h;

Reference yield:

: 83205-52-1,2080-86-6
3β-benzoyloxy-androst-5-en-17-one

: 135573-96-5
3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-methanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: aq. sodium hydrogen phosphate, aq. peroxyacetic acid / CHCl₃ / 2 h

2: 87 percent / 72percent aq. perchloric acid / dioxane; acetone / 3 h

3: 2.) H₂SO₄ / 1.) reflux, 2.) a) 30 deg C, 30 min, b) 20 deg C, 2 h

4: 82 percent / conc. HCl / methanol; CHCl₃ / 60 h / 35 °C

5: 90 percent / pyridine / 1 h / 0 °C

With pyridine; hydrogenchloride; peracetic acid; disodium hydrogenphosphate; perchloric acid; sulfuric acid; In 1,4-dioxane; methanol; chloroform; acetone;

Reference yield:

: 135573-93-2
3β,5,6β-trihydroxy-5α-androstan-17-one 3-benzoate

: 135573-96-5
3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) H₂SO₄ / 1.) reflux, 2.) a) 30 deg C, 30 min, b) 20 deg C, 2 h

2: 82 percent / conc. HCl / methanol; CHCl₃ / 60 h / 35 °C

3: 90 percent / pyridine / 1 h / 0 °C

With pyridine; hydrogenchloride; sulfuric acid; In methanol; chloroform;