4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α,9β,10β-androstan-3β-yl cyclohexanecarboxylate

Base Information

Chemical Name:4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α,9β,10β-androstan-3β-yl cyclohexanecarboxylate
CAS No.:200120-85-0
Molecular Formula:C₂₆H₄₀O₄
Molecular Weight:416.601
Hs Code.:

Synonyms:4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α,9β,10β-androstan-3β-yl cyclohexanecarboxylate

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Chemical Property of 4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α,9β,10β-androstan-3β-yl cyclohexanecarboxylate

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Technology Process of 4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α,9β,10β-androstan-3β-yl cyclohexanecarboxylate

There total 3 articles about 4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α,9β,10β-androstan-3β-yl cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 200120-84-9
4aα,17β-Dihydroxy-4aβ-methyl-4a-homo-7,19-dinor-5α,9β,10β-androstan-3β-yl cyclohexanecarboxylate

: 200120-85-0
4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α,9β,10β-androstan-3β-yl cyclohexanecarboxylate

Guidance literature:: With jones reagent; In acetone; at 0 ℃; for 0.166667h;
DOI:10.1135/cccc19971631

Reference yield:

: 135573-96-5
3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-methanesulfonate

: 200120-85-0
4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α,9β,10β-androstan-3β-yl cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / aq. CH₃COOK / acetone / 5 h / Heating

2: 63 percent / H₂ / Pt / acetic acid / 24 h / Ambient temperature

3: 69 percent / Jones reagent / acetone / 0.17 h / 0 °C

With jones reagent; hydrogen; potassium acetate; platinum; In acetic acid; acetone;
DOI:10.1135/cccc19971631

Reference yield:

: 200120-83-8
4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α-androst-9-en-3β-yl benzoate

: 200120-85-0
4aα-Hydroxy-4aβ-methyl-17-oxo-4a-homo-7,19-dinor-5α,9β,10β-androstan-3β-yl cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / H₂ / Pt / acetic acid / 24 h / Ambient temperature

2: 69 percent / Jones reagent / acetone / 0.17 h / 0 °C

With jones reagent; hydrogen; platinum; In acetic acid; acetone;
DOI:10.1135/cccc19971631