2-[4-(1,1-dimethylethyl)phenyl]-6-methylsulfamoyl-4H-3,1-benzoxazin-4-one

Base Information

Chemical Name:2-[4-(1,1-dimethylethyl)phenyl]-6-methylsulfamoyl-4H-3,1-benzoxazin-4-one
CAS No.:117145-63-8
Molecular Formula:C₁₉H₂₀N₂O₄S
Molecular Weight:372.445
Hs Code.:

Synonyms:2-[4-(1,1-dimethylethyl)phenyl]-6-methylsulfamoyl-4H-3,1-benzoxazin-4-one

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Chemical Property of 2-[4-(1,1-dimethylethyl)phenyl]-6-methylsulfamoyl-4H-3,1-benzoxazin-4-one

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Technology Process of 2-[4-(1,1-dimethylethyl)phenyl]-6-methylsulfamoyl-4H-3,1-benzoxazin-4-one

There total 4 articles about 2-[4-(1,1-dimethylethyl)phenyl]-6-methylsulfamoyl-4H-3,1-benzoxazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 124-63-0
methanesulfonyl chloride

: 117145-61-6
6-amino-2-[4-(1,1-dimethylethyl)phenyl]-4H-3,1-benzoxazin-4-one

: 117145-63-8
2-[4-(1,1-dimethylethyl)phenyl]-6-methylsulfamoyl-4H-3,1-benzoxazin-4-one

Guidance literature:: With pyridine; for 18h; Ambient temperature;
DOI:10.1021/jm00121a047

Reference yield:

: 117145-60-5
6-nitro-2-(4-t-butylphenyl)-4H-3,1-benzoxazin-4-one

: 117145-63-8
2-[4-(1,1-dimethylethyl)phenyl]-6-methylsulfamoyl-4H-3,1-benzoxazin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / H₂ / 5percent Pd/C / ethyl acetate / 1 h / 760 Torr

2: 56 percent / pyridine / 18 h / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1021/jm00121a047

Reference yield:

: 616-79-5
2-amino-5-nitro-benzoic acid

: 117145-63-8
2-[4-(1,1-dimethylethyl)phenyl]-6-methylsulfamoyl-4H-3,1-benzoxazin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / NEt₃ / dimethylformamide / 23 h / Ambient temperature

2: 62 percent / H₂ / 5percent Pd/C / ethyl acetate / 1 h / 760 Torr

3: 56 percent / pyridine / 18 h / Ambient temperature

With pyridine; hydrogen; triethylamine; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00121a047