Methyl 3-(8-(5,6-dimethoxypyridin-2-ylamino)-[1,2,4]-triazolo[1,5-a]pyridin-6-yl)benzoate

Base Information

Chemical Name:Methyl 3-(8-(5,6-dimethoxypyridin-2-ylamino)-[1,2,4]-triazolo[1,5-a]pyridin-6-yl)benzoate
CAS No.:1415695-13-4
Molecular Formula:C₂₁H₁₉N₅O₄
Molecular Weight:405.413
Hs Code.:

Synonyms:Methyl 3-(8-(5,6-dimethoxypyridin-2-ylamino)-[1,2,4]-triazolo[1,5-a]pyridin-6-yl)benzoate

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Chemical Property of Methyl 3-(8-(5,6-dimethoxypyridin-2-ylamino)-[1,2,4]-triazolo[1,5-a]pyridin-6-yl)benzoate

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Technology Process of Methyl 3-(8-(5,6-dimethoxypyridin-2-ylamino)-[1,2,4]-triazolo[1,5-a]pyridin-6-yl)benzoate

There total 11 articles about Methyl 3-(8-(5,6-dimethoxypyridin-2-ylamino)-[1,2,4]-triazolo[1,5-a]pyridin-6-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127980-46-5
5,6-dimethoxypyridin-2-amine

: 1415695-12-3
Methyl 3-(8-bromo-[1,2,4]-triazolo[1,5-a]pyridin-6-yl)benzoate

: 1415695-13-4
Methyl 3-(8-(5,6-dimethoxypyridin-2-ylamino)-[1,2,4]-triazolo[1,5-a]pyridin-6-yl)benzoate

Guidance literature:: With caesium carbonate; XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In 1,4-dioxane; at 20 - 96 ℃; for 24.16h; Inert atmosphere;

Reference yield:

: 480425-35-2
methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

: 1415695-01-0
6-chloro-N-(5,6-dimethoxypyridin-2-yl)-[1,2,4]-triazolo[1,5-a]pyridin-8-amine

: 1415695-13-4
Methyl 3-(8-(5,6-dimethoxypyridin-2-ylamino)-[1,2,4]-triazolo[1,5-a]pyridin-6-yl)benzoate

Guidance literature:: With sodium carbonate; XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In 1,4-dioxane; water; for 18h; Reflux; Inert atmosphere;

Reference yield:

: 20511-12-0
2-amino-5-iodopyridine

: 1415695-13-4
Methyl 3-(8-(5,6-dimethoxypyridin-2-ylamino)-[1,2,4]-triazolo[1,5-a]pyridin-6-yl)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-Bromosuccinimide / acetonitrile / 72 h / 20 °C

2.1: isopropyl alcohol / Inert atmosphere; Reflux

2.2: 50 °C

3.1: trifluoroacetic anhydride / tetrahydrofuran / 0 - 20 °C

3.2: pH 8

4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 24.25 h / 20 °C / Inert atmosphere; Reflux

5.1: caesium carbonate; XPhos / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 24.16 h / 20 - 96 °C / Inert atmosphere

With N-Bromosuccinimide; sodium carbonate; caesium carbonate; trifluoroacetic anhydride; XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; water; isopropyl alcohol; acetonitrile;