5-(p-benzyloxyphenyl)-5-hydroxy-4-oxohexanoic acid benzylamide

Base Information

Chemical Name:5-(p-benzyloxyphenyl)-5-hydroxy-4-oxohexanoic acid benzylamide
CAS No.:134734-44-4
Molecular Formula:C₂₆H₂₇NO₄
Molecular Weight:417.505
Hs Code.:

Synonyms:5-(p-benzyloxyphenyl)-5-hydroxy-4-oxohexanoic acid benzylamide

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Chemical Property of 5-(p-benzyloxyphenyl)-5-hydroxy-4-oxohexanoic acid benzylamide

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Technology Process of 5-(p-benzyloxyphenyl)-5-hydroxy-4-oxohexanoic acid benzylamide

There total 3 articles about 5-(p-benzyloxyphenyl)-5-hydroxy-4-oxohexanoic acid benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 134734-39-7
δ-(p-benzyloxyxyphenyl)-δ-methyl-δ-(γ-oxo)valerolactone

: 100-46-9
benzylamine

: 134734-44-4
5-(p-benzyloxyphenyl)-5-hydroxy-4-oxohexanoic acid benzylamide

Guidance literature:: With potassium cyanide; In methanol; at 55 ℃;
DOI:10.1002/jhet.5570280311

Reference yield:

: 106281-27-0
2-(p-benzyloxyphenyl)-6-hydroxy-2-methyl-2H-pyran-3(6H)-one

: 134734-44-4
5-(p-benzyloxyphenyl)-5-hydroxy-4-oxohexanoic acid benzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / CrO₃, conc. H₂SO₄, H₂O (Jones reagent) / acetone / 0.25 h

2: 95 percent / zinc dust / CHCl₃; acetic acid / 3 h / Ambient temperature

3: 82 percent / KCN / methanol / 55 °C

With chromium(VI) oxide; potassium cyanide; sulfuric acid; water; zinc; In methanol; chloroform; acetic acid; acetone;
DOI:10.1002/jhet.5570280311

Reference yield:

: 134734-37-5
δ-(p-benzyloxyxyphenyl)-δ-methyl-δ-(γ-oxo)crotonolactone

: 134734-44-4
5-(p-benzyloxyphenyl)-5-hydroxy-4-oxohexanoic acid benzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / zinc dust / CHCl₃; acetic acid / 3 h / Ambient temperature

2: 82 percent / KCN / methanol / 55 °C

With potassium cyanide; zinc; In methanol; chloroform; acetic acid;
DOI:10.1002/jhet.5570280311