2-[2-(1,3-dioxo-1,3-dihydroisoindol-2-yloxymethyl)phenyl]-3-methoxyacrylic acid methyl ester

Base Information

Chemical Name:2-[2-(1,3-dioxo-1,3-dihydroisoindol-2-yloxymethyl)phenyl]-3-methoxyacrylic acid methyl ester
CAS No.:139752-37-7
Molecular Formula:C₂₀H₁₇NO₆
Molecular Weight:367.358
Hs Code.:

Synonyms:2-[2-(1,3-dioxo-1,3-dihydroisoindol-2-yloxymethyl)phenyl]-3-methoxyacrylic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[2-(1,3-dioxo-1,3-dihydroisoindol-2-yloxymethyl)phenyl]-3-methoxyacrylic acid methyl ester

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Technology Process of 2-[2-(1,3-dioxo-1,3-dihydroisoindol-2-yloxymethyl)phenyl]-3-methoxyacrylic acid methyl ester

There total 2 articles about 2-[2-(1,3-dioxo-1,3-dihydroisoindol-2-yloxymethyl)phenyl]-3-methoxyacrylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.6%

: 117428-95-2
methyl 2-(2'-chloromethylphenyl)-3-methoxyacrylate

: 524-38-9
N-hydroxyphthalimide

: 139752-37-7
2-[2-(1,3-dioxo-1,3-dihydroisoindol-2-yloxymethyl)phenyl]-3-methoxyacrylic acid methyl ester

Guidance literature:: With sodium hydroxide; In N,N-dimethyl-formamide; at 80 ℃; for 2h;
DOI:10.1016/j.ejmech.2011.01.031

Reference yield:

: 85-44-9
phthalic anhydride

: 139752-37-7
2-[2-(1,3-dioxo-1,3-dihydroisoindol-2-yloxymethyl)phenyl]-3-methoxyacrylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; hydroxylamine hydrochloride

2: sodium hydroxide / N,N-dimethyl-formamide / 2 h / 80 °C

With pyridine; hydroxylamine hydrochloride; sodium hydroxide; In N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.01.031