6-(2,6-dimethyl-3,5-bis(methoxycarbonyl)-1,4-dihydropyrid-4-yl)-2,3-diphenylquinoxaline

Base Information

Chemical Name:6-(2,6-dimethyl-3,5-bis(methoxycarbonyl)-1,4-dihydropyrid-4-yl)-2,3-diphenylquinoxaline
CAS No.:121497-25-4
Molecular Formula:C₃₁H₂₇N₃O₄
Molecular Weight:505.573
Hs Code.:

Synonyms:6-(2,6-dimethyl-3,5-bis(methoxycarbonyl)-1,4-dihydropyrid-4-yl)-2,3-diphenylquinoxaline

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Chemical Property of 6-(2,6-dimethyl-3,5-bis(methoxycarbonyl)-1,4-dihydropyrid-4-yl)-2,3-diphenylquinoxaline

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Technology Process of 6-(2,6-dimethyl-3,5-bis(methoxycarbonyl)-1,4-dihydropyrid-4-yl)-2,3-diphenylquinoxaline

There total 4 articles about 6-(2,6-dimethyl-3,5-bis(methoxycarbonyl)-1,4-dihydropyrid-4-yl)-2,3-diphenylquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 134-81-6
benzil

: 121497-15-2
4-(3,4-diaminophenyl)-2,6-dimethyl-3,5-bis(methoxycarbonyl)-1,4-dihydropyridine

: 121497-25-4
6-(2,6-dimethyl-3,5-bis(methoxycarbonyl)-1,4-dihydropyrid-4-yl)-2,3-diphenylquinoxaline

Guidance literature:: In methanol; for 5h; Heating;
DOI:10.1021/jm00130a012

Reference yield:

: 51818-99-6
4-amino-3-nitro-benzaldehyde

: 121497-25-4
6-(2,6-dimethyl-3,5-bis(methoxycarbonyl)-1,4-dihydropyrid-4-yl)-2,3-diphenylquinoxaline

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / ethane-1,2-diol / 24 h / Heating

2: 72 percent / H₂ / Raney Ni / methanol / 2 h / 1838.8 Torr

3: 65 percent / methanol / 5 h / Heating

With hydrogen; nickel; In methanol; ethylene glycol;
DOI:10.1021/jm00130a012

Reference yield:

: 121497-08-3
4-(4-Amino-3-nitro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid dimethyl ester

: 121497-25-4
6-(2,6-dimethyl-3,5-bis(methoxycarbonyl)-1,4-dihydropyrid-4-yl)-2,3-diphenylquinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / H₂ / Raney Ni / methanol / 2 h / 1838.8 Torr

2: 65 percent / methanol / 5 h / Heating

With hydrogen; nickel; In methanol;
DOI:10.1021/jm00130a012