ethyl 10-phenylphenanthrene-9-carboxylate

Base Information

Chemical Name:ethyl 10-phenylphenanthrene-9-carboxylate
CAS No.:102593-53-3
Molecular Formula:C₂₃H₁₈O₂
Molecular Weight:326.395
Hs Code.:

Synonyms:ethyl 10-phenylphenanthrene-9-carboxylate

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Chemical Property of ethyl 10-phenylphenanthrene-9-carboxylate

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Technology Process of ethyl 10-phenylphenanthrene-9-carboxylate

There total 9 articles about ethyl 10-phenylphenanthrene-9-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 318-13-8
[1,1'-biphenyl]-2-diazonium tetrafluoroborate

: 2216-94-6
phenylpropynoic acid ethyl ester

: 102593-53-3
ethyl 10-phenylphenanthrene-9-carboxylate

Guidance literature:: With eosin; In acetonitrile; at 20 ℃; for 12h; Inert atmosphere; Irradiation;
DOI:10.1002/adsc.201200569

Reference yield: 38.0%

: 14002-52-9
o-phenylbenzoyl chloride

: 2216-94-6
phenylpropynoic acid ethyl ester

: 102593-53-3
ethyl 10-phenylphenanthrene-9-carboxylate

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; tri-tert-butyl phosphine; In o-xylene; at 160 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jo501835u

Reference yield: 31.0%

: 90-41-5
2-phenylaniline

: 2216-94-6
phenylpropynoic acid ethyl ester

: 92-52-4,1594-86-1
biphenyl

: 102593-53-3
ethyl 10-phenylphenanthrene-9-carboxylate

Guidance literature:: With fac-tris(2-phenylpyridinato-N,C₂')iridium(III); tert.-butylnitrite; In acetonitrile; at 20 ℃; Sealed tube; Irradiation;
DOI:10.1021/acs.joc.7b00413