2-(4-benzylphenyl)-3-cyano-1-((1R,2S)-2-((1,1-dimethylethyl)dimethylsilyloxy)-1-methyl-2-phenylethyl)-1-methylguanidine

Base Information

Chemical Name:2-(4-benzylphenyl)-3-cyano-1-((1R,2S)-2-((1,1-dimethylethyl)dimethylsilyloxy)-1-methyl-2-phenylethyl)-1-methylguanidine
CAS No.:353525-66-3
Molecular Formula:C₃₁H₄₀N₄OSi
Molecular Weight:512.77
Hs Code.:

Synonyms:2-(4-benzylphenyl)-3-cyano-1-((1R,2S)-2-((1,1-dimethylethyl)dimethylsilyloxy)-1-methyl-2-phenylethyl)-1-methylguanidine

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Chemical Property of 2-(4-benzylphenyl)-3-cyano-1-((1R,2S)-2-((1,1-dimethylethyl)dimethylsilyloxy)-1-methyl-2-phenylethyl)-1-methylguanidine

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Technology Process of 2-(4-benzylphenyl)-3-cyano-1-((1R,2S)-2-((1,1-dimethylethyl)dimethylsilyloxy)-1-methyl-2-phenylethyl)-1-methylguanidine

There total 3 articles about 2-(4-benzylphenyl)-3-cyano-1-((1R,2S)-2-((1,1-dimethylethyl)dimethylsilyloxy)-1-methyl-2-phenylethyl)-1-methylguanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 321-98-2,7009-81-6,90-83-5,6912-63-6
(1S,2R)-(+)-ephedrine

: 353525-66-3
2-(4-benzylphenyl)-3-cyano-1-((1R,2S)-2-((1,1-dimethylethyl)dimethylsilyloxy)-1-methyl-2-phenylethyl)-1-methylguanidine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / Et₃N; 4-(dimethylamino)pyridine / benzene; CH₂Cl₂ / 15 h / 20 °C

2: propan-2-ol / 2 h / Heating

With dmap; triethylamine; In dichloromethane; isopropyl alcohol; benzene;
DOI:10.1021/jm0004547

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 353525-66-3
2-(4-benzylphenyl)-3-cyano-1-((1R,2S)-2-((1,1-dimethylethyl)dimethylsilyloxy)-1-methyl-2-phenylethyl)-1-methylguanidine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / Et₃N; 4-(dimethylamino)pyridine / benzene; CH₂Cl₂ / 15 h / 20 °C

2: propan-2-ol / 2 h / Heating

With dmap; triethylamine; In dichloromethane; isopropyl alcohol; benzene;
DOI:10.1021/jm0004547

Reference yield:

: 1135-12-2
p-benzylaniline

: 353525-66-3
2-(4-benzylphenyl)-3-cyano-1-((1R,2S)-2-((1,1-dimethylethyl)dimethylsilyloxy)-1-methyl-2-phenylethyl)-1-methylguanidine

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / acetonitrile / 3 h / Heating

2: propan-2-ol / 2 h / Heating

In isopropyl alcohol; acetonitrile;
DOI:10.1021/jm0004547