Technology Process of C35H38N4O6
There total 8 articles about C35H38N4O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
piperidine;
In
ethanol;
at 65 - 80 ℃;
for 6h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: magnesium sulfate; sodium sulfate / dichloromethane / 72 h / 20 °C / Inert atmosphere
2: sodium tetrahydroborate; ethanol / tetrahydrofuran; ethanol / 0.5 h / 20 °C / Inert atmosphere
3: sodium hydrogencarbonate / tetrahydrofuran; water / 72 h / 20 °C
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 20 °C
5: pyridinium chlorochromate / dichloromethane / 1.5 h / 20 °C / Darkness
6: piperidine / ethanol / 6 h / 65 - 80 °C
With
piperidine; sodium tetrahydroborate; ethanol; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; magnesium sulfate; sodium sulfate; pyridinium chlorochromate;
In
tetrahydrofuran; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: platinum(IV) oxide; hydrogen / ethyl acetate / 4 h / 20 °C
2: magnesium sulfate; sodium sulfate / dichloromethane / 72 h / 20 °C / Inert atmosphere
3: sodium tetrahydroborate; ethanol / tetrahydrofuran; ethanol / 0.5 h / 20 °C / Inert atmosphere
4: sodium hydrogencarbonate / tetrahydrofuran; water / 72 h / 20 °C
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 20 °C
6: pyridinium chlorochromate / dichloromethane / 1.5 h / 20 °C / Darkness
7: piperidine / ethanol / 6 h / 65 - 80 °C
With
piperidine; platinum(IV) oxide; sodium tetrahydroborate; ethanol; tetrabutyl ammonium fluoride; hydrogen; sodium hydrogencarbonate; magnesium sulfate; sodium sulfate; pyridinium chlorochromate;
In
tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate;