trans-5-(trimethylsiloxy)-5,6-dihydro-3-phenyl-6-(trimethylsiloxy)-4H-1,2-oxazine

Base Information

Chemical Name:trans-5-(trimethylsiloxy)-5,6-dihydro-3-phenyl-6-(trimethylsiloxy)-4H-1,2-oxazine
CAS No.:124481-51-2
Molecular Formula:C₁₆H₂₇NO₃Si₂
Molecular Weight:337.566
Hs Code.:

Synonyms:trans-5-(trimethylsiloxy)-5,6-dihydro-3-phenyl-6-(trimethylsiloxy)-4H-1,2-oxazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-5-(trimethylsiloxy)-5,6-dihydro-3-phenyl-6-(trimethylsiloxy)-4H-1,2-oxazine

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Technology Process of trans-5-(trimethylsiloxy)-5,6-dihydro-3-phenyl-6-(trimethylsiloxy)-4H-1,2-oxazine

There total 2 articles about trans-5-(trimethylsiloxy)-5,6-dihydro-3-phenyl-6-(trimethylsiloxy)-4H-1,2-oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 6039-89-0
1,2-bis(trimethylsiloxy)ethene

: 21572-32-7
2-chloro-1-phenyl-ethanone oxime

: 124481-51-2
trans-5-(trimethylsiloxy)-5,6-dihydro-3-phenyl-6-(trimethylsiloxy)-4H-1,2-oxazine

Guidance literature:: With sodium carbonate; In diethyl ether; for 72h;

Reference yield:

: 26327-98-0
(Z)-2,2,7,7-tetramethyl-3,6-dioxa-2,7-disilaoct-4-ene

: 21572-32-7
2-chloro-1-phenyl-ethanone oxime

: 124481-51-2
trans-5-(trimethylsiloxy)-5,6-dihydro-3-phenyl-6-(trimethylsiloxy)-4H-1,2-oxazine

: 128388-80-7
(5R,6R)-3-Phenyl-5,6-bis-trimethylsilanyloxy-5,6-dihydro-4H-[1,2]oxazine

Guidance literature:: With sodium carbonate; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) diethyl ether, rt, 120 h;

Reference yield: 29.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 124481-51-2
trans-5-(trimethylsiloxy)-5,6-dihydro-3-phenyl-6-(trimethylsiloxy)-4H-1,2-oxazine

: 1243250-53-4
N-tert-butoxycarbonyl-4-hydroxy-2-phenylpyrrolidine

: 1243250-52-3
N-tert-butoxycarbonyl-2-phenyl-4-(trimethylsiloxy)pyrrolidine

: 913642-44-1
N-tert-butoxycarbonyl-1-amino-4-phenyl-2-butanol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; ethyl acetate; at 20 ℃; for 48h; under 760.051 Torr; Inert atmosphere;
DOI:10.1002/ejoc.201000425