ethyl (Z)-3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-ethoxypropenoate

Base Information

Chemical Name:ethyl (Z)-3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-ethoxypropenoate
CAS No.:305827-83-2
Molecular Formula:C₂₃H₂₅NO₆
Molecular Weight:411.455
Hs Code.:

Synonyms:ethyl (Z)-3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-ethoxypropenoate

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Chemical Property of ethyl (Z)-3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-ethoxypropenoate

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Technology Process of ethyl (Z)-3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-ethoxypropenoate

There total 1 articles about ethyl (Z)-3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-ethoxypropenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 216691-10-0
4-[2-(2,3-dihydro-benzo[1,4]oxazin-4-yl)-ethoxy]benzaldehyde

: 13676-06-7
ethyl 2-ethoxy-2-(diethylphosphono)acetate

: 305827-83-2
ethyl (Z)-3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-ethoxypropenoate

: 305827-81-0
ethyl (E)-3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-ethoxypropenoate

Guidance literature:: ethyl 2-ethoxy-2-(diethylphosphono)acetate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

4-[2-(2,3-dihydro-benzo[1,4]oxazin-4-yl)-ethoxy]benzaldehyde; In tetrahydrofuran; at 25 ℃; for 20h;

Reference yield: 64.0%

: 67-56-1
methanol

: 305827-83-2
ethyl (Z)-3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-ethoxypropenoate

: 223606-56-2,223606-57-3,223606-58-4
(+/-) Methyl 3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-ethoxypropanoate

Guidance literature:: methanol; ethyl (Z)-3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-ethoxypropenoate; With magnesium; at 25 ℃; for 20h;

With hydrogenchloride; In water; pH=~ 7;