acide 4-nitrobenzoique-14C

Base Information

• Chemical Name: acide 4-nitrobenzoique-14C
• CAS No.: 54744-98-8
• Molecular Formula: C₇H₅NO₄
• Molecular Weight: 169.11
• Mol file: 54744-98-8.mol

Synonyms:acide 4-nitrobenzoique-14C

Chemical Property of acide 4-nitrobenzoique-14C

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of acide 4-nitrobenzoique-14C

There total 5 articles about acide 4-nitrobenzoique-14C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

4-nitro-[α-14C]benzonitrile (115255-48-6) → acide 4-nitrobenzoique-14C (54744-98-8)

Guidance literature:

With water; sodium hydroxide; at 80 ℃; for 2h;

DOI:10.1002/jlcr.3403

Reference yield: 45.0%

C16(14)CH21N3O5 → acide 4-nitrobenzoique-14C (54744-98-8) + C7(14)CH7NO3

Guidance literature:

With hydrogenchloride; In water; at 125 ℃; for 16h;

DOI:10.1002/jlcr.3403

Reference yield:

p-nitrobenzene iodide (636-98-6) → acide 4-nitrobenzoique-14C (54744-98-8)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / Inert atmosphere; Heating

2: sodium hydroxide; water / 2 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; sodium hydroxide; In tetrahydrofuran;

DOI:10.1002/jlcr.3403

upstream raw materials:

4-nitro-[α-¹⁴C]benzonitrile

p-nitrobenzene iodide

4-nitro-[α-¹⁴C]benzoyl chloride

Downstream raw materials:

4-amino<7-14C>benzoic acid