2-[4'-(4''-hydroxy-phenylazo)-benzoylamino]-ethyl-carbamic acid tert-butyl ester

Base Information

• Chemical Name: 2-[4'-(4''-hydroxy-phenylazo)-benzoylamino]-ethyl-carbamic acid tert-butyl ester
• CAS No.: 1207289-77-7
• Molecular Formula: C₂₀H₂₄N₄O₄
• Molecular Weight: 384.435

Synonyms:2-[4'-(4''-hydroxy-phenylazo)-benzoylamino]-ethyl-carbamic acid tert-butyl ester

Chemical Property of 2-[4'-(4''-hydroxy-phenylazo)-benzoylamino]-ethyl-carbamic acid tert-butyl ester

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Technology Process of 2-[4'-(4''-hydroxy-phenylazo)-benzoylamino]-ethyl-carbamic acid tert-butyl ester

There total 1 articles about 2-[4'-(4''-hydroxy-phenylazo)-benzoylamino]-ethyl-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N-BOC-1,2-diaminoethane (57260-73-8) + 4-(4-hydroxphenylazo)benzoic acid (105299-45-4,2497-38-3) → 2-[4'-(4''-hydroxy-phenylazo)-benzoylamino]-ethyl-carbamic acid tert-butyl ester (1207289-77-7)

Guidance literature:

4-(4-hydroxphenylazo)benzoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; for 0.25h; Inert atmosphere;

N-BOC-1,2-diaminoethane; In N,N-dimethyl-formamide; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1039/b916693a

Reference yield: 67.0%

2-[4'-(4''-hydroxy-phenylazo)-benzoylamino]-ethyl-carbamic acid tert-butyl ester (1207289-77-7) + 1,3-dibromo-propane (109-64-8) → 2-{4'''-[4''-(3'-bromo-propoxy)-phenylazo]-benzoylamino}-ethyl-carbamic acid tert-butyl ester (1207289-69-7)

Guidance literature:

With potassium carbonate; In acetonitrile; for 5h; Reflux; Inert atmosphere;

DOI:10.1039/b916693a

upstream raw materials:

N-BOC-1,2-diaminoethane

4-(4-hydroxphenylazo)benzoic acid

Downstream raw materials:

2-{4'''-[4''-(3'-bromo-propoxy)-phenylazo]-benzoylamino}-ethyl-carbamic acid tert-butyl ester

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