des-methyl ceratamine B

Base Information

• Chemical Name: des-methyl ceratamine B
• CAS No.: 1152720-58-5
• Molecular Formula: C₁₅H₁₂Br₂N₄O₂
• Molecular Weight: 440.094
• Mol file: 1152720-58-5.mol

Synonyms:des-methyl ceratamine B

Chemical Property of des-methyl ceratamine B

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of des-methyl ceratamine B

There total 1 articles about des-methyl ceratamine B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

tetrahydro-des-methyl ceratamine B trifluoroacetic acid salt (1152720-57-4) → des-methyl ceratamine B (1152720-58-5)

Guidance literature:

With pyridine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 35 ℃; for 1h;

DOI:10.1021/ol900709n

Reference yield: 50.0%

des-methyl ceratamine B (1152720-58-5) + methyl iodide (74-88-4) → des-Methyl Ceratamine A (1152720-59-6)

Guidance literature:

des-methyl ceratamine B; With sodium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃;

methyl iodide; In tetrahydrofuran; N,N-dimethyl-formamide; at -78 - -10 ℃;

With water; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1021/ol900709n

upstream raw materials:

tetrahydro-des-methyl ceratamine B trifluoroacetic acid salt

Downstream raw materials:

des-Methyl Ceratamine A