benzyl 9H-fluoren-9-ylmethyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

Base Information

Chemical Name:benzyl 9H-fluoren-9-ylmethyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate
CAS No.:883981-61-1
Molecular Formula:C₃₅H₄₄N₂O₅
Molecular Weight:572.745
Hs Code.:

Synonyms:benzyl 9H-fluoren-9-ylmethyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

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Chemical Property of benzyl 9H-fluoren-9-ylmethyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

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Technology Process of benzyl 9H-fluoren-9-ylmethyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

There total 3 articles about benzyl 9H-fluoren-9-ylmethyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 883981-60-0
allyl benzyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

: 883981-61-1
benzyl 9H-fluoren-9-ylmethyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: phenylsilane; Pd(PPh₃)4 / CH₂Cl₂ / 0.75 h

2: 1.10 g / Et₃N / CH₂Cl₂ / 0.75 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane; triethylamine; In dichloromethane;
DOI:10.1021/ja057664z

Reference yield:

: 883981-58-6
dimethyl (5-{[(allyloxy)carbonyl]amino}pentyl)(5-{[(benzyloxy)carbonyl]amino}pentyl)malonate

: 883981-61-1
benzyl 9H-fluoren-9-ylmethyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / LiCl; water / dimethylsulfoxide / 4 h / 160 °C

2: 68 percent / diisobutylaluminum hydride / toluene; tetrahydrofuran / 4 h / -78 °C

3: phenylsilane; Pd(PPh₃)4 / CH₂Cl₂ / 0.75 h

4: 1.10 g / Et₃N / CH₂Cl₂ / 0.75 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane; water; diisobutylaluminium hydride; triethylamine; lithium chloride; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/ja057664z

Reference yield:

: 883981-59-7
methyl 7-{[(allyloxy)carbonyl]amino}-2-(5-{[(benzyloxy)carbonyl]amino}pentyl)heptanoate

: 883981-61-1
benzyl 9H-fluoren-9-ylmethyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / diisobutylaluminum hydride / toluene; tetrahydrofuran / 4 h / -78 °C

2: phenylsilane; Pd(PPh₃)4 / CH₂Cl₂ / 0.75 h

3: 1.10 g / Et₃N / CH₂Cl₂ / 0.75 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja057664z