allyl benzyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

Base Information

Chemical Name:allyl benzyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate
CAS No.:883981-60-0
Molecular Formula:C₂₄H₃₈N₂O₅
Molecular Weight:434.576
Hs Code.:

Synonyms:allyl benzyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

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Chemical Property of allyl benzyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

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Technology Process of allyl benzyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

There total 2 articles about allyl benzyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 883981-59-7
methyl 7-{[(allyloxy)carbonyl]amino}-2-(5-{[(benzyloxy)carbonyl]amino}pentyl)heptanoate

: 883981-60-0
allyl benzyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -78 ℃; for 4h;
DOI:10.1021/ja057664z

Reference yield:

: 883981-58-6
dimethyl (5-{[(allyloxy)carbonyl]amino}pentyl)(5-{[(benzyloxy)carbonyl]amino}pentyl)malonate

: 883981-60-0
allyl benzyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / LiCl; water / dimethylsulfoxide / 4 h / 160 °C

2: 68 percent / diisobutylaluminum hydride / toluene; tetrahydrofuran / 4 h / -78 °C

With water; diisobutylaluminium hydride; lithium chloride; In tetrahydrofuran; dimethyl sulfoxide; toluene;
DOI:10.1021/ja057664z

Reference yield:

: 883981-60-0
allyl benzyl [6-(hydroxymethyl)undecane-1,11-diyl]biscarbamate

: but-2-enedioic acid [11-amino-6-(tert-butyl-dimethyl-silanyloxymethyl)-undecyl]-amide (2,2-diphenyl-ethyl)-amide

Guidance literature:: Multi-step reaction with 6 steps

1.1: phenylsilane; Pd(PPh₃)4 / CH₂Cl₂ / 0.75 h

2.1: 1.10 g / Et₃N / CH₂Cl₂ / 0.75 h

3.1: H₂; HCl / Pd/C / diethyl ether; methanol / atmospheric pressure

4.1: 1-[3-dimethylaminopropyl]-3-ethylcarbodiimide hydrochloride; 1-hydroxybenzotriazole hydrate; triethylamine / CH₂Cl₂ / 0.5 h / 20 °C

4.2: 550 mg / triethylamine / CH₂Cl₂ / 4 h / 20 °C

5.1: 63 percent / imidazole / CH₂Cl₂ / 2 h

6.1: piperidine / tetrahydrofuran; acetonitrile / 2.5 h / 20 °C

With piperidine; 1H-imidazole; hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane; hydrogen; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/ja057664z