C₄₄H₇₆N₂O₁₃Si₄

Base Information

Chemical Name:C₄₄H₇₆N₂O₁₃Si₄
CAS No.:1127247-04-4
Molecular Formula:C₄₄H₇₆N₂O₁₃Si₄
Molecular Weight:953.435
Hs Code.:

C<sub>44</sub>H<sub>76</sub>N<sub>2</sub>O<sub>13</sub>Si<sub>4</sub>

Synonyms:C₄₄H₇₆N₂O₁₃Si₄

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Chemical Property of C₄₄H₇₆N₂O₁₃Si₄

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Technology Process of C₄₄H₇₆N₂O₁₃Si₄

There total 7 articles about C₄₄H₇₆N₂O₁₃Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1127247-03-3
C₃₇H₇₃NO₉Si₄

: 7693-46-1
4-Nitrophenyl chloroformate

: 1127247-04-4
C₄₄H₇₆N₂O₁₃Si₄

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 22h;

Reference yield:

: 3068-32-4
1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside

: 1127247-04-4
C₄₄H₇₆N₂O₁₃Si₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: silver(l) oxide / acetonitrile / 12 h / 20 °C / Darkness; Inert atmosphere

2.1: sodium tetrahydroborate / isopropyl alcohol; chloroform / 12 h / 0 - 20 °C / Inert atmosphere

3.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C

4.1: sodium methylate / methanol / 12 h / 20 °C

4.2: Dowex_.(R). H⁺ resin / pH 5

5.1: 1H-imidazole / dichloromethane / 12 h / 20 °C

6.1: trifluoroacetic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 22 h / 20 °C

With 1H-imidazole; dmap; sodium tetrahydroborate; sodium methylate; triethylamine; trifluoroacetic acid; silver(l) oxide; In methanol; dichloromethane; chloroform; isopropyl alcohol; acetonitrile;

Reference yield:

: 3011-34-5
4-hydroxy-3-nitrobenzaldehyde

: 1127247-04-4
C₄₄H₇₆N₂O₁₃Si₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: silver(l) oxide / acetonitrile / 12 h / 20 °C / Darkness; Inert atmosphere

2.1: sodium tetrahydroborate / isopropyl alcohol; chloroform / 12 h / 0 - 20 °C / Inert atmosphere

3.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C

4.1: sodium methylate / methanol / 12 h / 20 °C

4.2: Dowex_.(R). H⁺ resin / pH 5

5.1: 1H-imidazole / dichloromethane / 12 h / 20 °C

6.1: trifluoroacetic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 22 h / 20 °C

With 1H-imidazole; dmap; sodium tetrahydroborate; sodium methylate; triethylamine; trifluoroacetic acid; silver(l) oxide; In methanol; dichloromethane; chloroform; isopropyl alcohol; acetonitrile;