6-N-Benzyloxycarbonyl-1,2-O-isopropyliden-(1/2,3,4,6)-6-amino-3,4-epimino-1,2-cyclohexandiol

Base Information

Chemical Name:6-N-Benzyloxycarbonyl-1,2-O-isopropyliden-(1/2,3,4,6)-6-amino-3,4-epimino-1,2-cyclohexandiol
CAS No.:74342-56-6
Molecular Formula:C₁₇H₂₂N₂O₄
Molecular Weight:318.373
Hs Code.:

Synonyms:6-N-Benzyloxycarbonyl-1,2-O-isopropyliden-(1/2,3,4,6)-6-amino-3,4-epimino-1,2-cyclohexandiol

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Chemical Property of 6-N-Benzyloxycarbonyl-1,2-O-isopropyliden-(1/2,3,4,6)-6-amino-3,4-epimino-1,2-cyclohexandiol

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Technology Process of 6-N-Benzyloxycarbonyl-1,2-O-isopropyliden-(1/2,3,4,6)-6-amino-3,4-epimino-1,2-cyclohexandiol

There total 3 articles about 6-N-Benzyloxycarbonyl-1,2-O-isopropyliden-(1/2,3,4,6)-6-amino-3,4-epimino-1,2-cyclohexandiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 74342-55-5
1,3-Bis-N-(benzyloxycarbonyl)-5,6-O-isopropyliden-4-O-mesyl-2-desoxystreptamin

: 74342-56-6
6-N-Benzyloxycarbonyl-1,2-O-isopropyliden-(1/2,3,4,6)-6-amino-3,4-epimino-1,2-cyclohexandiol

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 5h;

Reference yield:

: 20399-15-9,31087-83-9,40896-00-2,40896-01-3
1,3-Bis-N-(benzyloxycarbonyl)-5,6-O-isopropyliden-2-desoxystreptamin

: 74342-56-6
6-N-Benzyloxycarbonyl-1,2-O-isopropyliden-(1/2,3,4,6)-6-amino-3,4-epimino-1,2-cyclohexandiol

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / pyridine / Ambient temperature

2: 1) NaH, 2) NH₄Cl / 1) DMF, 5 h

With pyridine; sodium hydride; ammonium chloride;