3-[(4-{[(4-bromophenyl)methylidene]amino}-5-thioxo-1,2,4-triazol-3-yl)methyl]-2(3H)-benzoxazolone

Base Information

Chemical Name:3-[(4-{[(4-bromophenyl)methylidene]amino}-5-thioxo-1,2,4-triazol-3-yl)methyl]-2(3H)-benzoxazolone
CAS No.:1428644-29-4
Molecular Formula:C₁₇H₁₂BrN₅O₂S
Molecular Weight:430.285
Hs Code.:

Synonyms:3-[(4-{[(4-bromophenyl)methylidene]amino}-5-thioxo-1,2,4-triazol-3-yl)methyl]-2(3H)-benzoxazolone

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Chemical Property of 3-[(4-{[(4-bromophenyl)methylidene]amino}-5-thioxo-1,2,4-triazol-3-yl)methyl]-2(3H)-benzoxazolone

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Technology Process of 3-[(4-{[(4-bromophenyl)methylidene]amino}-5-thioxo-1,2,4-triazol-3-yl)methyl]-2(3H)-benzoxazolone

There total 4 articles about 3-[(4-{[(4-bromophenyl)methylidene]amino}-5-thioxo-1,2,4-triazol-3-yl)methyl]-2(3H)-benzoxazolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-55-6
2-amino-phenol

: 1428644-29-4
3-[(4-{[(4-bromophenyl)methylidene]amino}-5-thioxo-1,2,4-triazol-3-yl)methyl]-2(3H)-benzoxazolone

Guidance literature:: Multi-step reaction with 5 steps

1: neat (no solvent) / Microwave irradiation

2: potassium carbonate / acetone / 0.25 h / 65 °C / Microwave irradiation

3: hydrogenchloride / water / 2 h / Reflux

4: 0.5 h / 160 - 170 °C

5: acetic acid / 125 °C / Microwave irradiation

With hydrogenchloride; potassium carbonate; acetic acid; In water; acetone;

Reference yield:

: 59-49-4
2-Benzoxazolinone

: 1428644-29-4
3-[(4-{[(4-bromophenyl)methylidene]amino}-5-thioxo-1,2,4-triazol-3-yl)methyl]-2(3H)-benzoxazolone

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 0.25 h / 65 °C / Microwave irradiation

2: hydrogenchloride / water / 2 h / Reflux

3: 0.5 h / 160 - 170 °C

4: acetic acid / 125 °C / Microwave irradiation

With hydrogenchloride; potassium carbonate; acetic acid; In water; acetone;

Reference yield:

: 13610-51-0
ethyl (2‐benzoxazolinone‐3‐yl)acetate

: 1428644-29-4
3-[(4-{[(4-bromophenyl)methylidene]amino}-5-thioxo-1,2,4-triazol-3-yl)methyl]-2(3H)-benzoxazolone

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / water / 2 h / Reflux

2: 0.5 h / 160 - 170 °C

3: acetic acid / 125 °C / Microwave irradiation

With hydrogenchloride; acetic acid; In water;